Julian-Tobias Schleich , Julius Max Jakob Siegmund , Minh Tien Phan , Philipp-Cornelius Pott , Hans Jürgen Maier , Christian Klose
{"title":"Co-extrusion of internally oxidized Nb-1Zr: An avenue to new load-bearing implants","authors":"Julian-Tobias Schleich , Julius Max Jakob Siegmund , Minh Tien Phan , Philipp-Cornelius Pott , Hans Jürgen Maier , Christian Klose","doi":"10.1016/j.mfglet.2026.02.003","DOIUrl":null,"url":null,"abstract":"<div><div>Niobium-zirconium alloys like Nb-1Zr offer high biocompatibility and osteoconductivity, with a lower Young’s modulus than Ti-6Al-4V, but their strength is limited due to a coarse grain structure. In this study, alloy strength is enhanced through controlled internal oxidation. Pre-oxidizing Nb-1Zr powder at 620 °C for 0, 60, and 120 min prior to co-extrusion increased 0.2% offset compression yield stress from 829 to 937 MPa. The improved strength is due to a fine-grained structure and high dislocation density. Longer oxidation times increased brittle niobium oxides. Future work will refine oxidation to tailor the properties of these alloys for load-bearing implants.</div></div>","PeriodicalId":38186,"journal":{"name":"Manufacturing Letters","volume":"47 ","pages":"Pages 74-77"},"PeriodicalIF":2.0000,"publicationDate":"2026-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Manufacturing Letters","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2213846326000052","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2026/2/12 0:00:00","PubModel":"Epub","JCR":"Q3","JCRName":"ENGINEERING, MANUFACTURING","Score":null,"Total":0}
引用次数: 0
Abstract
Niobium-zirconium alloys like Nb-1Zr offer high biocompatibility and osteoconductivity, with a lower Young’s modulus than Ti-6Al-4V, but their strength is limited due to a coarse grain structure. In this study, alloy strength is enhanced through controlled internal oxidation. Pre-oxidizing Nb-1Zr powder at 620 °C for 0, 60, and 120 min prior to co-extrusion increased 0.2% offset compression yield stress from 829 to 937 MPa. The improved strength is due to a fine-grained structure and high dislocation density. Longer oxidation times increased brittle niobium oxides. Future work will refine oxidation to tailor the properties of these alloys for load-bearing implants.