Effect of surface treatments on shear bond strength between CAD/CAM glass fiber-reinforced composite block and veneering indirect composite material.

IF 1.8 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE
Dental materials journal Pub Date : 2026-03-29 Epub Date: 2026-03-05 DOI:10.4012/dmj.2025-185
Satomi Arai, Kei Kubochi, Keisuke Hoshino, Daishi Nakase, Ralf J Kohal, Futoshi Komine
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Abstract

This study aimed to evaluate the effect of different surface treatments and artificial aging on the shear bond strength between a CAD/CAM glass fiber-reinforced composite (FRC) block and a veneering indirect composite material. Four surface treatments-no surface treatment (NT), airborne-particle abrasion (AB), tribochemical silica coating (ROC), and hydrofluoric acid etching (HF)-were assessed with and without silane application. Specimens were subjected to thermocycling and mechanical loading to simulate aging. Shear bond strength was measured, and failure modes were analyzed using scanning electron microscopy and energy-dispersive X-ray spectroscopy. The AB group exhibited the highest bond strength without silane application. The ROC group combined with silane yielded the highest bond strength, particularly after thermal cycling. Mechanical loading reduced the effectiveness of silane application. These findings indicate that tribochemical silica coating followed by silanization provides a superior and durable bond between FRC blocks and veneering indirect composite materials.

表面处理对CAD/CAM玻璃纤维增强复合块与贴面间接复合材料剪切粘结强度的影响
本研究旨在评估不同表面处理和人工老化对CAD/CAM玻璃纤维增强复合材料(FRC)砌块与贴面间接复合材料之间剪切结合强度的影响。四种表面处理——无表面处理(NT)、空气颗粒磨损(AB)、摩擦化学二氧化硅涂层(ROC)和氢氟酸蚀刻(HF)——在有和没有硅烷应用的情况下进行了评估。试样进行了热循环和机械加载模拟老化。采用扫描电镜和能量色散x射线能谱分析了剪切粘结强度和破坏模式。在不添加硅烷的情况下,AB基团的结合强度最高。ROC基团与硅烷结合产生了最高的键强度,特别是在热循环之后。机械负荷降低了硅烷应用的有效性。这些发现表明,摩擦化学二氧化硅涂层之后的硅烷化为FRC块和贴面间接复合材料之间提供了优越而持久的粘合。
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来源期刊
Dental materials journal
Dental materials journal 医学-材料科学:生物材料
CiteScore
4.60
自引率
4.00%
发文量
102
审稿时长
3 months
期刊介绍: Dental Materials Journal is a peer review journal published by the Japanese Society for Dental Materials and Devises aiming to introduce the progress of the basic and applied sciences in dental materials and biomaterials. The dental materials-related clinical science and instrumental technologies are also within the scope of this journal. The materials dealt include synthetic polymers, ceramics, metals and tissue-derived biomaterials. Forefront dental materials and biomaterials used in developing filed, such as tissue engineering, bioengineering and artificial intelligence, are positively considered for the review as well. Recent acceptance rate of the submitted manuscript in the journal is around 30%.
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