First Repeatability and Reproducibility Indicators for the ISO 13785-1/NPR 6999 Intermediate-Scale Façade Test

IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
Eric Guillaume, Guillaume Le-Goff, Bauke Knottnerus, Talal Fateh
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Abstract

This short communication reports the preliminary repeatability and reproducibility (R&R) results for the intermediate-scale façade test in accordance with ISO 13785-1/NPR 6999. A three-laboratory round-robin was conducted on two cladding systems (a phenolic foam system, K15B, and a wood panel), and complemented by an intra-laboratory repeatability series on a second phenolic formulation (K15N). Three output metrics were assessed: the 60-s running-average peak heat release rate (HRR60s av, max) and total heat released at 5 and 30 min (THR5, THR30). Data were treated under the ISO 5725 and ISO 13528 frameworks with a limited dataset; inter-laboratory standard deviations were pooled across sites, Z-scores were used to screen for outliers, and, where multi-site repeats were not feasible, the within-site repeatability standard deviation was proxied by a single intralaboratory series. Across both products, THR-based metrics exhibited lower repeatability than HRR60s av, max, with repeatability consistently tighter than inter-laboratory reproducibility, and no |Z| ≥ 2 observations. Reproducibility is better for HRR60s av, max, but further data will be required to refine these trends. Practical guard bands derived from the pooled coefficients of variation are proposed to support method qualification and acceptance criteria. The findings also inform the ongoing revision of ISO 13785-1, which now contemplates explicit HRR measurement, and highlight the role of intermediate-scale testing as a cost-effective bridge between small-scale screening and full-scale façade performance assessment, providing a tool for extensions of applications. Limitations due to small sample sizes are noted, and recommendations are given for future r&R campaigns.

ISO 13785-1/NPR 6999中等规模表面测试的第一个重复性和再现性指标
本简短通信报告了根据ISO 13785-1/NPR 6999进行的中等规模farade试验的初步重复性和再现性(R&;R)结果。对两种覆层系统(酚醛泡沫系统,K15B和木板)进行了三个实验室的循环测试,并对第二种酚醛配方(K15N)进行了实验室内的可重复性测试。评估了三个输出指标:60秒运行时的平均峰值放热率(HRR60s av, max)和5和30分钟的总放热率(THR5, THR30)。数据在有限数据集的ISO 5725和ISO 13528框架下处理;实验室间标准偏差汇集在一起,z分数用于筛选异常值,当多位点重复不可行的情况下,实验室内重复性标准偏差由单个实验室内序列代替。在这两种产品中,基于hr的指标的重复性低于HRR60s的av, max,重复性始终比实验室间的重复性更严格,并且没有|Z|≥2的观察值。HRR60s的可重复性较好,但需要进一步的数据来完善这些趋势。提出了由汇总变异系数推导出的实用保护带,以支持方法鉴定和验收准则。这些发现还为正在进行的ISO 13785-1修订提供了信息,该修订现在考虑了明确的HRR测量,并强调了中等规模测试作为小规模筛选和全面farade性能评估之间的经济有效桥梁的作用,为扩展应用提供了工具。注意到由于样本量小而造成的局限性,并对未来的研发活动提出了建议。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Fire and Materials
Fire and Materials 工程技术-材料科学:综合
CiteScore
4.60
自引率
5.30%
发文量
72
审稿时长
3 months
期刊介绍: Fire and Materials is an international journal for scientific and technological communications directed at the fire properties of materials and the products into which they are made. This covers all aspects of the polymer field and the end uses where polymers find application; the important developments in the fields of natural products - wood and cellulosics; non-polymeric materials - metals and ceramics; as well as the chemistry and industrial applications of fire retardant chemicals. Contributions will be particularly welcomed on heat release; properties of combustion products - smoke opacity, toxicity and corrosivity; modelling and testing.
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