Influence of the Degree of HPT Deformation on the Microstructural Characteristics and Mechanical Properties of the Zn–4Ag–1Cu Alloy

IF 0.4 4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING
M. V. Polenok, E. D. Khafizova, R. K. Islamgaliev, R. K. Nafikov, E. D. Abdrakhmanova, Kunxia Wei, Wei Wei
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Abstract

This study investigated the microstructure and mechanical properties of a Zn–4Ag–1Cu (wt %) alloy processed by high-pressure torsion (HPT) at room temperature through 1 to 10 turns. Microstructural analysis reveals that HPT processing results in the formation of a homogeneous ultrafine-grained (UFG) structure in the alloy samples, with a grain size ranging from 250 to 600 nm, containing nanoscale particles of secondary phases. In the early stages of deformation, after HPT with 1 to 10 turns, a significant increase in strength properties is observed in the UFG samples compared to the initial state. The yield stress and ultimate tensile strength reach 165 and 236 MPa, respectively. An increase in the number of HPT turns from 1 to 10 is accompanied by a decrease in strength and a notable increase in the plasticity of the samples. The elongation to failure increases by an order of magnitude, from 13 to 112 and 250%. Experimental data confirm the manifestation of grain boundary sliding and dynamic recrystallization effects, leading to a significant increase in the plasticity of the UFG alloy at room temperature. This study demonstrates the high efficiency of using the HPT method to form a UFG structure in the Zn–4% Ag–1% Cu alloy, which provides a combination of properties attractive for bioresorbable implants and stents used in medicine.

Abstract Image

HPT变形程度对Zn-4Ag-1Cu合金组织特征和力学性能的影响
研究了室温高压扭转(HPT) 1 ~ 10匝Zn-4Ag-1Cu (wt %)合金的组织和力学性能。显微组织分析表明,HPT处理使合金样品形成了均匀的超细晶(UFG)组织,晶粒尺寸在250 ~ 600 nm之间,含有纳米级二次相颗粒。在变形的早期阶段,经过1到10圈的高温拉伸后,与初始状态相比,在UFG样品中观察到强度特性的显著增加。屈服应力和极限抗拉强度分别达到165和236 MPa。当HPT匝数从1次增加到10次时,试样的强度降低,塑性显著提高。断裂伸长率增加了一个数量级,从13%增加到112%和250%。实验数据证实了晶界滑动和动态再结晶效应的表现,导致UFG合金在室温下塑性显著提高。这项研究证明了使用HPT方法在Zn-4% Ag-1% Cu合金中形成UFG结构的高效率,这为医学上使用的生物可吸收植入物和支架提供了具有吸引力的性能组合。
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来源期刊
Russian Journal of Non-Ferrous Metals
Russian Journal of Non-Ferrous Metals METALLURGY & METALLURGICAL ENGINEERING-
CiteScore
1.90
自引率
12.50%
发文量
59
审稿时长
3 months
期刊介绍: Russian Journal of Non-Ferrous Metals is a journal the main goal of which is to achieve new knowledge in the following topics: extraction metallurgy, hydro- and pirometallurgy, casting, plastic deformation, metallography and heat treatment, powder metallurgy and composites, self-propagating high-temperature synthesis, surface engineering and advanced protected coatings, environments, and energy capacity in non-ferrous metallurgy.
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