Preparation and Investigation of Composite Based on Reduced Graphene Oxide and Fe3O4 Nanoparticles

IF 1.5 3区 化学 Q3 CHEMISTRY, INORGANIC & NUCLEAR
V. R. Ibragimova, I. V. Sapkov, E. I. Efremova, Z. A. Kudryashova, E. G. Rustamova, D. V. Korolev, E. I. Kunitsyna, Yu. V. Ioni
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Abstract

Graphene oxide (GO) and composites based on it are often used to produce graphene-like materials by thermal or chemical reduction, and the reduction method strongly affects the properties of the materials. In this study, a new method was proposed to prepare a conductive composite based on reduced graphene oxide (rGO) with magnetite nanoparticles (NPs) with an average diameter of 18 nm dispersed on its surface. The method consisted of treating a GO-based composite with Fe3O4 on the its surface in supercritical isopropanol. The composites based on GO and rGO and magnetite NPs were investigated by FTIR spectroscopy, X-ray powder diffraction analysis, and scanning electron microscopy. It is shown that the sample compact film of the rGO-based composite has specific surface resistivity is 22 Ω cm–2 and saturation magnetisation is 32.3 emu/g.

Abstract Image

还原性氧化石墨烯与纳米Fe3O4复合材料的制备与研究
氧化石墨烯(GO)及其复合材料常用于通过热还原或化学还原制备类石墨烯材料,而还原方法对材料的性能影响很大。本研究提出了一种以还原氧化石墨烯(rGO)为基础,表面分散平均直径为18 nm的磁铁矿纳米颗粒(NPs)制备导电复合材料的新方法。该方法是在超临界异丙醇中处理氧化石墨烯基复合材料,表面有Fe3O4。采用红外光谱、x射线粉末衍射和扫描电镜对氧化石墨烯、还原氧化石墨烯和磁铁矿NPs复合材料进行了表征。结果表明,rgo基复合材料的致密膜样品的比表面电阻率为22 Ω cm-2,饱和磁化强度为32.3 emu/g。
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来源期刊
Russian Journal of Inorganic Chemistry
Russian Journal of Inorganic Chemistry 化学-无机化学与核化学
CiteScore
3.10
自引率
38.10%
发文量
237
审稿时长
3 months
期刊介绍: Russian Journal of Inorganic Chemistry is a monthly periodical that covers the following topics of research: the synthesis and properties of inorganic compounds, coordination compounds, physicochemical analysis of inorganic systems, theoretical inorganic chemistry, physical methods of investigation, chemistry of solutions, inorganic materials, and nanomaterials.
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