Preparation of a Rolled Thin Sheet from a Molybdenum Single Crystal while Maintaining a Single-Crystal Structure

IF 0.3 Q4 METALLURGY & METALLURGICAL ENGINEERING
N. B. Kolchugina, N. A. Dormidontov, V. M. Kirillova, R. D. Karelin, V. V. Sdobyrev, A. S. Bakulina, V. N. Serebryanyi, A. S. Kolyanova, R. A. Vakhrushev, S. V. Gorbunov
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Abstract

Manufacturing foundations for maintaining a single-crystal structure in rolled thin sheets (0.5 mm thick) prepared from a high-purity [110] molybdenum single crystal grown by electron-beam zone melting are reported. The sheets are manufactured from plate workpieces cut from the single crystal using cold rolling (350°C); a reduction per pass of 5, 10, and 15% to a total strain of 50–75%; and intermediate and final annealing. The maximum scatter of the [001] orientation in the rolled sheets is 3.42°; after final annealing, it is 2.64°. The substructure is studied, and the microhardnesses of the single-crystal plate workpieces (≈177 HV0.5), the final-thickness rolled sheets (≈199 HV0.5), and the sheets subjected to final annealing (≈190 HV0.5) are estimated.

Abstract Image

在保持单晶结构的情况下用钼单晶制备轧制薄板
本文报道了用电子束区熔炼生长的高纯度[110]钼单晶制备的轧制薄板(0.5 mm厚)保持单晶结构的制造基础。薄板是用冷轧(350°C)从单晶切割的板工件制造的;每道次减少5%、10%和15%,总应变为50-75%;中间退火和最终退火。[001]取向在轧制薄板中的最大散射角为3.42°;最终退火后为2.64°。研究了子结构,并对单晶板工件(≈177 HV0.5)、终轧薄板(≈199 HV0.5)和终退火薄板(≈190 HV0.5)的显微硬度进行了估计。
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来源期刊
Russian Metallurgy (Metally)
Russian Metallurgy (Metally) METALLURGY & METALLURGICAL ENGINEERING-
CiteScore
0.70
自引率
25.00%
发文量
140
期刊介绍: Russian Metallurgy (Metally)  publishes results of original experimental and theoretical research in the form of reviews and regular articles devoted to topical problems of metallurgy, physical metallurgy, and treatment of ferrous, nonferrous, rare, and other metals and alloys, intermetallic compounds, and metallic composite materials. The journal focuses on physicochemical properties of metallurgical materials (ores, slags, matters, and melts of metals and alloys); physicochemical processes (thermodynamics and kinetics of pyrometallurgical, hydrometallurgical, electrochemical, and other processes); theoretical metallurgy; metal forming; thermoplastic and thermochemical treatment; computation and experimental determination of phase diagrams and thermokinetic diagrams; mechanisms and kinetics of phase transitions in metallic materials; relations between the chemical composition, phase and structural states of materials and their physicochemical and service properties; interaction between metallic materials and external media; and effects of radiation on these materials.
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