Recent perspectives of microplastic analysis from sampling to characterization

Foysal Mahmud , Hridoy Roy , Mustafa Md Wasif , Abir Mahmud , Md. Nymuzzaman Saikat , Addrita Haque , Eduardo Alberto Lopez-Maldonado , Abul Basar Baki , Md. Shahinoor Islam
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Abstract

Microplastic (MP) pollution has been an emerging global concern due to its persistent nature and the requirement for sophisticated detection techniques. However, MP research has always been complexified due to the unavailability of structured methodology and the ambiguity of process selection. This review has critically analyzed different aspects of MP abundance in water, sediments, biota and wastewater and MP analyzing techniques. MP analysis results are solely dependent on its processing stages, such as oven drying and sieving, chemical digestion, and alkaline treatment, which are the crucial parts of MP sample preparation and processing. To identify the specified polymer in MP samples, analytical techniques such as Fourier transform infrared Spectroscopy (FTIR), Raman spectra (RS), and pyrolysis-gas chromatography-mass spectrometry (Pyr GC-MS) are widely used. Among the applied techniques, FTIR is the cheapest, whereas µ-RS is the most accurate. MP matrix specifications and concentrations vary for water, sediments, biota, and wastewater sources. The highest concentration of 152,688 ± 92,384 particles/m3 MP was observed for the Sea Surface Microlayer of 1000 µm. The MPs concentration in river water reached 718 ± 244 MPs/m3. River sediments of developing countries like Bangladesh, Indonesia and Taiwan have very high concentrations of MPs, which is a great concern for river biota. Various types of plastics, including PP, PE, PE-PP, PE-PDM, PET, nylon, T-elastomer, CP, wool, and cotton, were identified in reported studies. The study discloses recent perspectives on MP research and appropriate sampling and analysis techniques are crucial for reporting MPs in environmental samples.
从取样到表征的微塑性分析的最新观点
微塑料污染由于其持久性和对复杂检测技术的要求,已成为一个新兴的全球关注的问题。然而,由于缺乏结构化的方法和过程选择的模糊性,MP研究一直是复杂的。本文从水体、沉积物、生物群和废水中MP丰度的不同方面以及MP分析技术进行了综述。MP分析结果完全取决于其处理阶段,如烘箱干燥和筛分、化学消解和碱性处理,这些是MP样品制备和处理的关键部分。为了鉴定MP样品中的特定聚合物,傅立叶变换红外光谱(FTIR)、拉曼光谱(RS)和热解-气相色谱-质谱(Pyr GC-MS)等分析技术被广泛使用。在应用的技术中,FTIR是最便宜的,而µrs是最准确的。MP基质规格和浓度因水、沉积物、生物群和废水来源而异。1000 µm海面微层最高浓度为152,688 ± 92,384粒/m3 MP。河水中MPs浓度达到718 ± 244 MPs/m3。各种类型的塑料,包括PP、PE、PE-PP、PE- pdm、PET、尼龙、t -弹性体、CP、羊毛和棉花,在报告的研究中被确定。该研究揭示了MP研究的最新观点,适当的采样和分析技术对于报告环境样本中的MP至关重要。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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