Kui Suo , Ziyu Pan , Lifeng Pan , Yabin Feng , Cunshan Zhou , Liyu Shi , Baoguo Xu , Yiting Guo , Zhenfeng Yang
{"title":"Freeze-thaw cycle synergistic pulsed light pretreatment improves vacuum freeze drying of Chinese bayberry","authors":"Kui Suo , Ziyu Pan , Lifeng Pan , Yabin Feng , Cunshan Zhou , Liyu Shi , Baoguo Xu , Yiting Guo , Zhenfeng Yang","doi":"10.1016/j.ifset.2025.104228","DOIUrl":null,"url":null,"abstract":"<div><div>Conventional drying methods for fruits and vegetables often struggle to balance drying efficiency, product quality, and energy consumption. To overcome these limitations, this study innovatively developed three-step strategy for Chinese bayberry drying, integrating three freeze-thaw cycles (FTC) pretreatment, pulsed light (PL; 1000 mJ/cm<sup>2</sup>, 6 cm, 15 flashes) pretreatment, and variable-temperature vacuum freeze-drying (VT-VFD; ramping from −20 °C to 25 °C). The results demonstrated that FTC (by enhancing porosity, connectivity, and permeability) combined with VT-VFD (by dynamic temperature rise), synergistically accelerated the drying process. Compared to constant-temperature VFD at −18 °C, 4 °C, and 25 °C, this combined approach reduced drying time by 11.32–72.19 % and energy consumption by 4.64–68.10 %. Additionally, it improved brittleness and reduced volume shrinkage, although it had a negative impact on color. Subsequent PL pretreatment effectively mitigated FTC induced color deterioration by inhibiting PPO and POD activities, reducing the <em>ΔE</em> value to 1.62, which closely approaches that of fresh samples. Moreover, compared to VT-VFD alone, the combined application of FTC and PL pretreatments yielded a “dual enhancement” in the retention of bioactive compounds and antioxidant capacity. Specifically, the retention rates of total phenolics, anthocyanins, and ascorbic acid increased by 37.97 %, 43.19 %, and 27.21 %, respectively, while DPPH and ABTS radical scavenging activities improved by 26.92 % and 49.16 %, respectively. Finally, PL pretreatment also enhanced microbial safety, reducing total bacterial by 0.93 log CFU/g and mold & yeast by 1.81 log CFU/g. By integrating physical field pretreatments with dynamic temperature-controlled drying, this study provides a broadly applicable model for the precision drying of other perishable fruits and vegetables.</div></div>","PeriodicalId":329,"journal":{"name":"Innovative Food Science & Emerging Technologies","volume":"105 ","pages":"Article 104228"},"PeriodicalIF":6.8000,"publicationDate":"2025-09-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Innovative Food Science & Emerging Technologies","FirstCategoryId":"97","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1466856425003121","RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"FOOD SCIENCE & TECHNOLOGY","Score":null,"Total":0}
引用次数: 0
Abstract
Conventional drying methods for fruits and vegetables often struggle to balance drying efficiency, product quality, and energy consumption. To overcome these limitations, this study innovatively developed three-step strategy for Chinese bayberry drying, integrating three freeze-thaw cycles (FTC) pretreatment, pulsed light (PL; 1000 mJ/cm2, 6 cm, 15 flashes) pretreatment, and variable-temperature vacuum freeze-drying (VT-VFD; ramping from −20 °C to 25 °C). The results demonstrated that FTC (by enhancing porosity, connectivity, and permeability) combined with VT-VFD (by dynamic temperature rise), synergistically accelerated the drying process. Compared to constant-temperature VFD at −18 °C, 4 °C, and 25 °C, this combined approach reduced drying time by 11.32–72.19 % and energy consumption by 4.64–68.10 %. Additionally, it improved brittleness and reduced volume shrinkage, although it had a negative impact on color. Subsequent PL pretreatment effectively mitigated FTC induced color deterioration by inhibiting PPO and POD activities, reducing the ΔE value to 1.62, which closely approaches that of fresh samples. Moreover, compared to VT-VFD alone, the combined application of FTC and PL pretreatments yielded a “dual enhancement” in the retention of bioactive compounds and antioxidant capacity. Specifically, the retention rates of total phenolics, anthocyanins, and ascorbic acid increased by 37.97 %, 43.19 %, and 27.21 %, respectively, while DPPH and ABTS radical scavenging activities improved by 26.92 % and 49.16 %, respectively. Finally, PL pretreatment also enhanced microbial safety, reducing total bacterial by 0.93 log CFU/g and mold & yeast by 1.81 log CFU/g. By integrating physical field pretreatments with dynamic temperature-controlled drying, this study provides a broadly applicable model for the precision drying of other perishable fruits and vegetables.
期刊介绍:
Innovative Food Science and Emerging Technologies (IFSET) aims to provide the highest quality original contributions and few, mainly upon invitation, reviews on and highly innovative developments in food science and emerging food process technologies. The significance of the results either for the science community or for industrial R&D groups must be specified. Papers submitted must be of highest scientific quality and only those advancing current scientific knowledge and understanding or with technical relevance will be considered.