{"title":"Preparation of fine-grained WC-4Co cemented carbides cutting tools with engineered surface micro-features by SPS and performance analysis","authors":"Sheng Wang, Zhenhua Wang, Linyan Liu, Daqin Tang, Chaohui Yin, Xin Shangguan","doi":"10.1016/j.ijrmhm.2025.107435","DOIUrl":null,"url":null,"abstract":"<div><div>WC-Co cemented carbides, renowned for their excellent wear resistance and impact toughness, are considered ideal materials for cutting tools. A novel rapid preparation method based on spark plasma sintering (SPS) is introduced to efficiently produce fine-grained cemented carbide cutting tools with engineered surface micro-features. The effects of compaction parameters (compaction pressure, holding time) and sintering parameters (sintering temperature, dwell time) on the microstructure, mechanical properties, and shape retention were systematically investigated in WC-4Co fine-grained cemented carbides. The results demonstrate that compaction at 3.0 × 10<sup>3</sup> kg with a 60-min holding time optimized green density (53.67 %) and shape fidelity (>90 %), thereby preventing crack formation induced by high pressure and extended duration. Sintering at 1350 °C for 10 min yielded optimal overall properties (hardness: 19.12 GPa; fracture toughness: 8.47 MPa·m<sup>1/2</sup>) while effectively suppressing abnormal WC grain growth. The η phase (Co<sub>3</sub>W<sub>3</sub>C) was found to accumulate exclusively on the surface and could be effectively eliminated through polishing. Turning experiments show that the main cutting force, feed force, passive force and cutting temperature of micro texture tools are reduced by 4.95–14.58 %, 13.35–26.72 %, 7.65–27.25 % and 4.21–9.82 % respectively compared with non-texture tools. The micro-texture on the front cutting surface also effectively prevents the formation of chip accumulation. This research provides both a theoretical foundation and technical support for the efficient production of high-performance micro-textured cutting tools.</div></div>","PeriodicalId":14216,"journal":{"name":"International Journal of Refractory Metals & Hard Materials","volume":"134 ","pages":"Article 107435"},"PeriodicalIF":4.6000,"publicationDate":"2025-09-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Refractory Metals & Hard Materials","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0263436825004007","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
Abstract
WC-Co cemented carbides, renowned for their excellent wear resistance and impact toughness, are considered ideal materials for cutting tools. A novel rapid preparation method based on spark plasma sintering (SPS) is introduced to efficiently produce fine-grained cemented carbide cutting tools with engineered surface micro-features. The effects of compaction parameters (compaction pressure, holding time) and sintering parameters (sintering temperature, dwell time) on the microstructure, mechanical properties, and shape retention were systematically investigated in WC-4Co fine-grained cemented carbides. The results demonstrate that compaction at 3.0 × 103 kg with a 60-min holding time optimized green density (53.67 %) and shape fidelity (>90 %), thereby preventing crack formation induced by high pressure and extended duration. Sintering at 1350 °C for 10 min yielded optimal overall properties (hardness: 19.12 GPa; fracture toughness: 8.47 MPa·m1/2) while effectively suppressing abnormal WC grain growth. The η phase (Co3W3C) was found to accumulate exclusively on the surface and could be effectively eliminated through polishing. Turning experiments show that the main cutting force, feed force, passive force and cutting temperature of micro texture tools are reduced by 4.95–14.58 %, 13.35–26.72 %, 7.65–27.25 % and 4.21–9.82 % respectively compared with non-texture tools. The micro-texture on the front cutting surface also effectively prevents the formation of chip accumulation. This research provides both a theoretical foundation and technical support for the efficient production of high-performance micro-textured cutting tools.
期刊介绍:
The International Journal of Refractory Metals and Hard Materials (IJRMHM) publishes original research articles concerned with all aspects of refractory metals and hard materials. Refractory metals are defined as metals with melting points higher than 1800 °C. These are tungsten, molybdenum, chromium, tantalum, niobium, hafnium, and rhenium, as well as many compounds and alloys based thereupon. Hard materials that are included in the scope of this journal are defined as materials with hardness values higher than 1000 kg/mm2, primarily intended for applications as manufacturing tools or wear resistant components in mechanical systems. Thus they encompass carbides, nitrides and borides of metals, and related compounds. A special focus of this journal is put on the family of hardmetals, which is also known as cemented tungsten carbide, and cermets which are based on titanium carbide and carbonitrides with or without a metal binder. Ceramics and superhard materials including diamond and cubic boron nitride may also be accepted provided the subject material is presented as hard materials as defined above.