Self-propagating high-temperature synthesis of Ca3N2 with improved nitriding degree and product composition

IF 0.4 4区物理与天体物理 Q4 PHYSICS, MULTIDISCIPLINARY

Russian Physics Journal Pub Date : 2025-07-31 DOI:10.1007/s11182-025-03502-3

A. N. Avramchik, O. A. Shkoda

引用次数: 0

Abstract

The paper deals with calcium nitride obtained by combustion synthesis of calcium metal pellets in nitrogen at a pressure of 3 to 7 MPa. The nitriding degree for calcium is about 99%. The obtained product composition is investigated by chemical and X-ray diffraction analyses. It is found that α‑ and β‑Ca₃N₂ phases are the primary in the product. Impurity phases include the Ca₂N phase, calcium nitrate and nitrite, and others.

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自蔓延高温合成提高氮化程度和产品成分的Ca3N2

本文研究了在3 ~ 7 MPa压力下，用氮气燃烧合成金属钙球团制得氮化钙。钙的氮化度约为99%。用化学分析和x射线衍射分析研究了所得产物的组成。α -和β - Ca3N2相是产物的主要相。杂质相包括Ca2N相、硝酸钙和亚硝酸盐等。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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来源期刊

Russian Physics Journal PHYSICS, MULTIDISCIPLINARY-

CiteScore

1.00

自引率

50.00%

发文量

208

审稿时长

3-6 weeks

期刊介绍： Russian Physics Journal covers the broad spectrum of specialized research in applied physics, with emphasis on work with practical applications in solid-state physics, optics, and magnetism. Particularly interesting results are reported in connection with: electroluminescence and crystal phospors; semiconductors; phase transformations in solids; superconductivity; properties of thin films; and magnetomechanical phenomena.