Performance verification of the "ghost"-free tomographic reconstruction method QURT

IF 2.2 3区 工程技术 Q1 MICROSCOPY
Norio Baba , Hiroyuki Ishikawa , Miki Ito
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引用次数: 0

Abstract

We recently proposed a novel tomographic reconstruction method called the quantisation unit reconstruction technique (QURT) that reconstructs a tomogram by arranging grey-level quantisation units in three-dimensional image space through unique discrete processing. QURT significantly reduces artificial image “ghost” generation caused by the “missing-wedge” and the number of projection images, which are common limitations of conventional methods. Unlike other recently developed advanced methods, such as compressed sensing, QURT does not require any parameter adjustments or modeling based on prior knowledge but requires only a series of projection images and tilt-angle data. It does not select the processing target because it exploits the inherent constraints of projection theory. In this study, the practical performance and resolution of QURT were quantitatively evaluated in both real and frequency domains using Fourier ring correlation and other metrics in simulations with fine test patterns. Even in the presence of the missing-wedge, QURT generated almost no ghost image outside the test pattern region, considerably suppressing the artifacts. This advanced property was experimentally validated by applying HAADF-STEM tomography to analyse a catalyst sample (Pd/CeO2–ZrO2–Al2O3), which was particularly sensitive to ghost image generation inside pores. QURT clearly revealed the pore structure without compromising the low-contrast Al regions and without generating ghost images, even at a tilt step angle of up to 4°. In EDXS tomography, QURT also reconstructed a 3D elemental map even from a small number of 22 tilt series signal maps with the missing-wedges.
无虚影层析重建方法QURT的性能验证
我们最近提出了一种新的层析重建方法,称为量化单元重建技术(QURT),该技术通过独特的离散处理,在三维图像空间中排列灰度量化单元来重建层析图。QURT显著减少了由于“缺楔”和投影图像数量而产生的人工图像“鬼影”,这是传统方法常见的局限性。与最近开发的其他先进方法(如压缩感知)不同,QURT不需要任何基于先验知识的参数调整或建模,而只需要一系列投影图像和倾角数据。由于利用了投影理论的固有约束,它没有选择处理目标。在本研究中,使用傅立叶环相关和其他指标在实域和频域对QURT的实际性能和分辨率进行了定量评估。即使在缺失的楔形存在的情况下,QURT在测试模式区域之外几乎没有生成鬼像,相当程度地抑制了伪影。通过HAADF-STEM断层扫描分析催化剂样品(Pd/ CeO2-ZrO2-Al2O3),实验验证了这种先进的特性,该样品对孔隙内产生的鬼像特别敏感。即使在高达4°的倾斜步进角下,QURT也能清晰地显示孔隙结构,而不会影响低对比度Al区域,也不会产生鬼影。在EDXS层析成像中,QURT还重建了一个三维元素图,甚至从22个少量的倾斜序列信号图中缺失楔形。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Micron
Micron 工程技术-显微镜技术
CiteScore
4.30
自引率
4.20%
发文量
100
审稿时长
31 days
期刊介绍: Micron is an interdisciplinary forum for all work that involves new applications of microscopy or where advanced microscopy plays a central role. The journal will publish on the design, methods, application, practice or theory of microscopy and microanalysis, including reports on optical, electron-beam, X-ray microtomography, and scanning-probe systems. It also aims at the regular publication of review papers, short communications, as well as thematic issues on contemporary developments in microscopy and microanalysis. The journal embraces original research in which microscopy has contributed significantly to knowledge in biology, life science, nanoscience and nanotechnology, materials science and engineering.
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