One-pot synthesis of silver-hydroxyapatite nanocomposites for sunscreens against high-energy visible light radiation

IF 2.7 4区材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY

Materials Letters Pub Date : 2025-06-20 DOI:10.1016/j.matlet.2025.138973

Jinutda Engsuwan , Sulawan Kaowphong , Sutinee Girdthep , Nawapong Chumha

引用次数: 0

Abstract

Silver-hydroxyapatite (AgHAP) nanocomposites were synthesized by a one-pot microwave irradiation method. AgHAP consisted of hydroxyapatite with a hexagonal structure and metallic silver (Ag⁰) with a cubic structure. The crystallinity of hydroxyapatite phase and UV radiation absorption capability of AgHAP improved with prolonged microwave irradiation times. The hydroxyapatite in AgHAP formed nanorods (50–100 nm), while Ag⁰ were nanoparticles (10–25 nm). The sunscreen containing AgHAP with a prolonged irradiation time of 60 cycles (AgHAP60) exhibited the highest sun protection factor (SPF) of 7.08 ± 0.85. The porphyrin protection factor (PPF) of the AgHAP samples was approximately 8.26 to 8.64. Furthermore, the minimum inhibitory concentration (MIC) and minimum bactericidal concentration (MBC) of AgHAP were 25 mg/ml.

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抗高能可见光辐射防晒霜用银-羟基磷灰石纳米复合材料的一锅合成

采用微波一锅法合成了银羟基磷灰石（AgHAP）纳米复合材料。AgHAP由六方结构的羟基磷灰石和立方结构的金属银（Ag0）组成。随着微波辐照时间的延长，AgHAP的羟基磷灰石相结晶度和紫外辐射吸收能力提高。AgHAP中羟基磷灰石形成纳米棒（50 ~ 100 nm），而Ag0为纳米颗粒（10 ~ 25 nm）。含AgHAP的防晒霜，当辐照时间延长60次（AgHAP60）时，其防晒系数（SPF）最高，为7.08±0.85。AgHAP样品的卟啉保护因子（PPF）约为8.26 ~ 8.64。AgHAP的最低抑菌浓度（MIC）和最低杀菌浓度（MBC）均为25 mg/ml。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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来源期刊

Materials Letters 工程技术-材料科学：综合

CiteScore

5.60

自引率

3.30%

发文量

1948

审稿时长

50 days

期刊介绍： Materials Letters has an open access mirror journal Materials Letters: X, sharing the same aims and scope, editorial team, submission system and rigorous peer review. Materials Letters is dedicated to publishing novel, cutting edge reports of broad interest to the materials community. The journal provides a forum for materials scientists and engineers, physicists, and chemists to rapidly communicate on the most important topics in the field of materials. Contributions include, but are not limited to, a variety of topics such as: • Materials - Metals and alloys, amorphous solids, ceramics, composites, polymers, semiconductors • Applications - Structural, opto-electronic, magnetic, medical, MEMS, sensors, smart • Characterization - Analytical, microscopy, scanning probes, nanoscopic, optical, electrical, magnetic, acoustic, spectroscopic, diffraction • Novel Materials - Micro and nanostructures (nanowires, nanotubes, nanoparticles), nanocomposites, thin films, superlattices, quantum dots. • Processing - Crystal growth, thin film processing, sol-gel processing, mechanical processing, assembly, nanocrystalline processing. • Properties - Mechanical, magnetic, optical, electrical, ferroelectric, thermal, interfacial, transport, thermodynamic • Synthesis - Quenching, solid state, solidification, solution synthesis, vapor deposition, high pressure, explosive