Low frequency band pass Fourier filtering for irradiation damage analysis in the transmission electron microscope

IF 2.2 3区 工程技术 Q1 MICROSCOPY
Daniel L. Foley , Emily H. Mang , Yongqiang Wang , Douglas E. Spearot , Mitra L. Taheri
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引用次数: 0

Abstract

We demonstrate a simple technique for improved imaging of non-crystallographic, irradiation-induced defects in the transmission electron microscope (TEM). By Fourier filtering bright-field TEM images to isolate relatively low-frequency fluctuations in intensity, it is possible to better resolve defects such as cavities caused by He-ion irradiation of iron. This analysis can be done with basic TEM imaging and most image processing software. This technique requires minimal defocus and can eliminate contrast mechanisms on both longer and short length scales. The resulting images are sensitive to filtering parameters, but clearly reveal the size, density, and distribution of cavities when compared with standard imaging techniques.
低频带通傅立叶滤波用于透射电镜辐照损伤分析
我们展示了一种简单的技术,用于改进透射电子显微镜(TEM)中非晶体,辐照诱导缺陷的成像。通过傅里叶滤波来隔离相对低频的强度波动,可以更好地解决由铁的氦离子辐照引起的空洞等缺陷。这种分析可以用基本的TEM成像和大多数图像处理软件来完成。这种技术需要最小的散焦,并且可以在较长和较短的长度尺度上消除对比度机制。所得图像对滤波参数很敏感,但与标准成像技术相比,可以清楚地显示空腔的大小、密度和分布。
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来源期刊
Micron
Micron 工程技术-显微镜技术
CiteScore
4.30
自引率
4.20%
发文量
100
审稿时长
31 days
期刊介绍: Micron is an interdisciplinary forum for all work that involves new applications of microscopy or where advanced microscopy plays a central role. The journal will publish on the design, methods, application, practice or theory of microscopy and microanalysis, including reports on optical, electron-beam, X-ray microtomography, and scanning-probe systems. It also aims at the regular publication of review papers, short communications, as well as thematic issues on contemporary developments in microscopy and microanalysis. The journal embraces original research in which microscopy has contributed significantly to knowledge in biology, life science, nanoscience and nanotechnology, materials science and engineering.
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