Daniel L. Foley , Emily H. Mang , Yongqiang Wang , Douglas E. Spearot , Mitra L. Taheri
{"title":"Low frequency band pass Fourier filtering for irradiation damage analysis in the transmission electron microscope","authors":"Daniel L. Foley , Emily H. Mang , Yongqiang Wang , Douglas E. Spearot , Mitra L. Taheri","doi":"10.1016/j.micron.2025.103864","DOIUrl":null,"url":null,"abstract":"<div><div>We demonstrate a simple technique for improved imaging of non-crystallographic, irradiation-induced defects in the transmission electron microscope (TEM). By Fourier filtering bright-field TEM images to isolate relatively low-frequency fluctuations in intensity, it is possible to better resolve defects such as cavities caused by He-ion irradiation of iron. This analysis can be done with basic TEM imaging and most image processing software. This technique requires minimal defocus and can eliminate contrast mechanisms on both longer and short length scales. The resulting images are sensitive to filtering parameters, but clearly reveal the size, density, and distribution of cavities when compared with standard imaging techniques.</div></div>","PeriodicalId":18501,"journal":{"name":"Micron","volume":"196 ","pages":"Article 103864"},"PeriodicalIF":2.2000,"publicationDate":"2025-06-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Micron","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0968432825000824","RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MICROSCOPY","Score":null,"Total":0}
引用次数: 0
Abstract
We demonstrate a simple technique for improved imaging of non-crystallographic, irradiation-induced defects in the transmission electron microscope (TEM). By Fourier filtering bright-field TEM images to isolate relatively low-frequency fluctuations in intensity, it is possible to better resolve defects such as cavities caused by He-ion irradiation of iron. This analysis can be done with basic TEM imaging and most image processing software. This technique requires minimal defocus and can eliminate contrast mechanisms on both longer and short length scales. The resulting images are sensitive to filtering parameters, but clearly reveal the size, density, and distribution of cavities when compared with standard imaging techniques.
期刊介绍:
Micron is an interdisciplinary forum for all work that involves new applications of microscopy or where advanced microscopy plays a central role. The journal will publish on the design, methods, application, practice or theory of microscopy and microanalysis, including reports on optical, electron-beam, X-ray microtomography, and scanning-probe systems. It also aims at the regular publication of review papers, short communications, as well as thematic issues on contemporary developments in microscopy and microanalysis. The journal embraces original research in which microscopy has contributed significantly to knowledge in biology, life science, nanoscience and nanotechnology, materials science and engineering.