An Overview of Thermal Methods Within the Analytical Framework of Cultural Heritage Studies.

IF 4.2 2区 化学 Q1 CHEMISTRY, ANALYTICAL
Mina Magdy
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引用次数: 0

Abstract

The article offers an overview of thermal methods in the field of heritage conservation and research. Thermal analysis encompasses a family of analytical methods in which the property of a sample is monitored to gain a deeper understanding of material properties under various thermal conditions. Thermal methods can provide profound insights into the thermal behavior of heritage materials, including thermogravimetric analysis (TGA), differential thermal analysis (DTA), differential scanning calorimetry (DSC), thermo-mechanical analysis (TMA), thermodilatometric analysis (TDA), dynamic mechanical analysis (DMA), dielectric thermal analysis (DETA), thermal conductivity (TC), infrared thermography (IRT), and thermoluminescence (TL). These methods serve as a valuable means of recording thermal events across a broad range of temperatures, such as glass transition temperature, melting temperature, crystallization temperature, specific heat capacity, thermal expansion coefficient, thermal curing, thermal shrinkage, TC, and thermal imaging. Combining multiple methods in a single measurement enhances the collection of more information simultaneously. Thermo-kinetic parameters play a crucial role in interpreting the results obtained from thermal analysis to predict the behavior of materials at different temperatures and understand the underlying mechanisms driving thermal transformations. The key advantage of thermal analysis practice is to answer questions regarding materials performance, materials selection, conservation treatments, and preventive measures.

文化遗产研究分析框架中的热方法综述。
本文概述了热方法在文物保护和研究领域的应用。热分析包括一系列分析方法,其中监测样品的性质,以更深入地了解各种热条件下的材料性质。热分析方法包括热重分析(TGA)、差热分析(DTA)、差热扫描量热法(DSC)、热力学分析(TMA)、热模拟分析(TDA)、动态力学分析(DMA)、介电热分析(DETA)、导热系数(TC)、红外热成像(IRT)和热释光(TL)等,可以深入了解文物材料的热行为。这些方法是记录各种温度范围内的热事件的有价值的手段,如玻璃化温度、熔化温度、结晶温度、比热容、热膨胀系数、热固化、热收缩、TC和热成像。在一次测量中结合多种方法可以同时收集更多的信息。热动力学参数在解释热分析结果以预测材料在不同温度下的行为和理解驱动热转化的潜在机制方面起着至关重要的作用。热分析实践的主要优势是回答有关材料性能、材料选择、保护处理和预防措施的问题。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
CiteScore
12.00
自引率
4.00%
发文量
137
审稿时长
6 months
期刊介绍: Critical Reviews in Analytical Chemistry continues to be a dependable resource for both the expert and the student by providing in-depth, scholarly, insightful reviews of important topics within the discipline of analytical chemistry and related measurement sciences. The journal exclusively publishes review articles that illuminate the underlying science, that evaluate the field''s status by putting recent developments into proper perspective and context, and that speculate on possible future developments. A limited number of articles are of a "tutorial" format written by experts for scientists seeking introduction or clarification in a new area. This journal serves as a forum for linking various underlying components in broad and interdisciplinary means, while maintaining balance between applied and fundamental research. Topics we are interested in receiving reviews on are the following: · chemical analysis; · instrumentation; · chemometrics; · analytical biochemistry; · medicinal analysis; · forensics; · environmental sciences; · applied physics; · and material science.
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