{"title":"Effect of boriding on wear and fatigue life of WC-Co die inserts in cold forming","authors":"Kubra Ozturk Guler , Bahadir Uyulgan , Burak Hizli , Umut Ince","doi":"10.1016/j.engfailanal.2025.109762","DOIUrl":null,"url":null,"abstract":"<div><div>Cold forging is a key manufacturing process in fastener production, utilizing multi-stage die systems to plastically deform materials under high compressive stresses. In cold forming operations such as extrusion, reduction, and head forming, WC-Co materials are widely employed in die applications, selected based on the specific requirements of the process. These die materials used in cold forming must exhibit high wear resistance and fatigue strength due to the substantial forming forces that generate significant stresses within the dies. Boriding, a surface treatment method, is applied to enhance these mechanical properties. This study investigates the effects of pack-boriding treatment on the fatigue life and wear properties of WC-Co material containing 19 % Co, which are used as die inserts in cold forging die systems. Three sets of samples were pack-borided using EKABOR-2 boron powder at 1000 °C, 950 °C, and 900 °C for 4 h under each temperature condition to accomplish this process. Following the pack-boriding process, pin-on-plate wear tests were conducted under both non-lubricated and lubricated conditions to evaluate the wear performance of the samples. Three-point bending fatigue tests were performed to assess the fatigue behavior of the borided samples. After the fatigue test, Goodman-Haigh diagrams were obtained from the experimental results to be utilized in predictive die-life calculations. X-ray diffraction (XRD) analysis confirmed the formation of CoB, Co<sub>2</sub>B, WB<sub>2</sub> and W<sub>2</sub>CoB<sub>2</sub> phases in the borided layer. Results indicate that increasing boriding temperature significantly improves wear resistance and surface hardness, with the highest microhardness (4104 HV<sub>0</sub>.<sub>1</sub>) and the lowest wear track width (183 µm non-lubricated, 70.76 µm lubricated) measured at 1000 °C. However, the thick and brittle boride layer induced stress concentrations, negatively affecting the material’s fatigue performance. According to the Goodman-Haigh diagrams, the highest fatigue life after boriding was measured as 5,000,000 cycles at 950 °C, while the lowest was 135,356 cycles at 450 MPa after boriding at 1000 °C. Although the increased hardness of the WB<sub>2</sub> phase at 1000 °C enhanced wear resistance, the formation of a brittle boride layer led to stress concentrations, facilitating crack initiation and reducing die life. This indicates that while higher boriding temperatures improve surface hardness, they also increase brittleness, negatively impacting the material’s fatigue performance.</div></div>","PeriodicalId":11677,"journal":{"name":"Engineering Failure Analysis","volume":"179 ","pages":"Article 109762"},"PeriodicalIF":4.4000,"publicationDate":"2025-05-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Engineering Failure Analysis","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1350630725005035","RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"ENGINEERING, MECHANICAL","Score":null,"Total":0}
引用次数: 0
Abstract
Cold forging is a key manufacturing process in fastener production, utilizing multi-stage die systems to plastically deform materials under high compressive stresses. In cold forming operations such as extrusion, reduction, and head forming, WC-Co materials are widely employed in die applications, selected based on the specific requirements of the process. These die materials used in cold forming must exhibit high wear resistance and fatigue strength due to the substantial forming forces that generate significant stresses within the dies. Boriding, a surface treatment method, is applied to enhance these mechanical properties. This study investigates the effects of pack-boriding treatment on the fatigue life and wear properties of WC-Co material containing 19 % Co, which are used as die inserts in cold forging die systems. Three sets of samples were pack-borided using EKABOR-2 boron powder at 1000 °C, 950 °C, and 900 °C for 4 h under each temperature condition to accomplish this process. Following the pack-boriding process, pin-on-plate wear tests were conducted under both non-lubricated and lubricated conditions to evaluate the wear performance of the samples. Three-point bending fatigue tests were performed to assess the fatigue behavior of the borided samples. After the fatigue test, Goodman-Haigh diagrams were obtained from the experimental results to be utilized in predictive die-life calculations. X-ray diffraction (XRD) analysis confirmed the formation of CoB, Co2B, WB2 and W2CoB2 phases in the borided layer. Results indicate that increasing boriding temperature significantly improves wear resistance and surface hardness, with the highest microhardness (4104 HV0.1) and the lowest wear track width (183 µm non-lubricated, 70.76 µm lubricated) measured at 1000 °C. However, the thick and brittle boride layer induced stress concentrations, negatively affecting the material’s fatigue performance. According to the Goodman-Haigh diagrams, the highest fatigue life after boriding was measured as 5,000,000 cycles at 950 °C, while the lowest was 135,356 cycles at 450 MPa after boriding at 1000 °C. Although the increased hardness of the WB2 phase at 1000 °C enhanced wear resistance, the formation of a brittle boride layer led to stress concentrations, facilitating crack initiation and reducing die life. This indicates that while higher boriding temperatures improve surface hardness, they also increase brittleness, negatively impacting the material’s fatigue performance.
期刊介绍:
Engineering Failure Analysis publishes research papers describing the analysis of engineering failures and related studies.
Papers relating to the structure, properties and behaviour of engineering materials are encouraged, particularly those which also involve the detailed application of materials parameters to problems in engineering structures, components and design. In addition to the area of materials engineering, the interacting fields of mechanical, manufacturing, aeronautical, civil, chemical, corrosion and design engineering are considered relevant. Activity should be directed at analysing engineering failures and carrying out research to help reduce the incidences of failures and to extend the operating horizons of engineering materials.
Emphasis is placed on the mechanical properties of materials and their behaviour when influenced by structure, process and environment. Metallic, polymeric, ceramic and natural materials are all included and the application of these materials to real engineering situations should be emphasised. The use of a case-study based approach is also encouraged.
Engineering Failure Analysis provides essential reference material and critical feedback into the design process thereby contributing to the prevention of engineering failures in the future. All submissions will be subject to peer review from leading experts in the field.