Júlia Dal Paz, Felipe Gomes Dallepiane, Alef da Silva, Lílian Vanessa Rossa Beltrami, William Haupt, Micheline Sandini Trentin
{"title":"Effects of corrosion on orthodontic mini-implants related to removal torque fracture resistance.","authors":"Júlia Dal Paz, Felipe Gomes Dallepiane, Alef da Silva, Lílian Vanessa Rossa Beltrami, William Haupt, Micheline Sandini Trentin","doi":"10.4317/jced.62447","DOIUrl":null,"url":null,"abstract":"<p><strong>Background: </strong>This study evaluated the effect of metallic corrosion on the torsional fracture resistance of mini-implants of different alloys in two solutions: artificial saliva and artificial saliva+fluoride.</p><p><strong>Material and methods: </strong>The research included 60 mini-implants: 30 of Ti6Al4V and 30 of stainless steel from the brand Morelli. The groups were divided into G1: stainless steel control, G2: Ti6Al4V control, G3: stainless steel in saliva, G4: stainless steel in saliva+fluoride, G5: Ti6Al4V in saliva, and G6: Ti6Al4V in saliva+fluoride, all with n=10. A potentiostat conducted electrochemical corrosion tests. Subsequently, one mini-implant from each group underwent SEM analysis for corrosion examination (80 and 5.000x). Then, the mini-implants were removed from the rods and subjected to a mechanical torsion fracture test (500N) using a mandrel coupled to a universal mechanical testing machine. After fracture or deformation, one mini-implant from each group underwent SEM analysis again (80 and 5.000x).</p><p><strong>Results: </strong>The statistical analysis showed no significant differences between the groups (stainless steel: 0.076 and Ti6Al4V: 0.199; p<i>p</i>>0.05). The Shapiro-Wilk test indicated that the data did not follow a normal distribution (<i>p</i><0.05). The pitting potential analysis revealed no significant differences between G3 and G4, G5 and G6, or G4 and G6. Fracture resistance tests showed that most stainless steel mini-implants deformed rather than fractured completely (G1: 33.95N; G3: 40.60N; G4: 28.26N), requiring higher force for fracture. All Ti6Al4V mini-implants fractured at lower forces due to the material's brittleness (G2: 26.35N; G5: 27.50N; G6: 24.01N).</p><p><strong>Conclusions: </strong>All analyzed groups experienced corrosion and pitting potentials, but none exerted sufficient influence to fracture or deform the devices under torsion. <b>Key words:</b>Mini-implants, corrosion, artificial saliva, fluoride, fracture resistance.</p>","PeriodicalId":15376,"journal":{"name":"Journal of Clinical and Experimental Dentistry","volume":"17 3","pages":"e273-e279"},"PeriodicalIF":0.0000,"publicationDate":"2025-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC11994201/pdf/","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Clinical and Experimental Dentistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.4317/jced.62447","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"Dentistry","Score":null,"Total":0}
引用次数: 0
Abstract
Background: This study evaluated the effect of metallic corrosion on the torsional fracture resistance of mini-implants of different alloys in two solutions: artificial saliva and artificial saliva+fluoride.
Material and methods: The research included 60 mini-implants: 30 of Ti6Al4V and 30 of stainless steel from the brand Morelli. The groups were divided into G1: stainless steel control, G2: Ti6Al4V control, G3: stainless steel in saliva, G4: stainless steel in saliva+fluoride, G5: Ti6Al4V in saliva, and G6: Ti6Al4V in saliva+fluoride, all with n=10. A potentiostat conducted electrochemical corrosion tests. Subsequently, one mini-implant from each group underwent SEM analysis for corrosion examination (80 and 5.000x). Then, the mini-implants were removed from the rods and subjected to a mechanical torsion fracture test (500N) using a mandrel coupled to a universal mechanical testing machine. After fracture or deformation, one mini-implant from each group underwent SEM analysis again (80 and 5.000x).
Results: The statistical analysis showed no significant differences between the groups (stainless steel: 0.076 and Ti6Al4V: 0.199; pp>0.05). The Shapiro-Wilk test indicated that the data did not follow a normal distribution (p<0.05). The pitting potential analysis revealed no significant differences between G3 and G4, G5 and G6, or G4 and G6. Fracture resistance tests showed that most stainless steel mini-implants deformed rather than fractured completely (G1: 33.95N; G3: 40.60N; G4: 28.26N), requiring higher force for fracture. All Ti6Al4V mini-implants fractured at lower forces due to the material's brittleness (G2: 26.35N; G5: 27.50N; G6: 24.01N).
Conclusions: All analyzed groups experienced corrosion and pitting potentials, but none exerted sufficient influence to fracture or deform the devices under torsion. Key words:Mini-implants, corrosion, artificial saliva, fluoride, fracture resistance.
期刊介绍:
Indexed in PUBMED, PubMed Central® (PMC) since 2012 and SCOPUSJournal of Clinical and Experimental Dentistry is an Open Access (free access on-line) - http://www.medicinaoral.com/odo/indice.htm. The aim of the Journal of Clinical and Experimental Dentistry is: - Periodontology - Community and Preventive Dentistry - Esthetic Dentistry - Biomaterials and Bioengineering in Dentistry - Operative Dentistry and Endodontics - Prosthetic Dentistry - Orthodontics - Oral Medicine and Pathology - Odontostomatology for the disabled or special patients - Oral Surgery