Leonarda Vugrin, Christos Chatzigiannis, Evelina Colacino and Ivan Halasz
{"title":"In situ Raman spectroscopy for comparing ball milling and resonant acoustic mixing in organic mechanosynthesis†","authors":"Leonarda Vugrin, Christos Chatzigiannis, Evelina Colacino and Ivan Halasz","doi":"10.1039/D5MR00016E","DOIUrl":null,"url":null,"abstract":"<p >By using <em>in situ</em> Raman spectroscopy for reaction monitoring, we compare ball milling (BM) and resonant acoustic mixing (RAM) in the preparation α,β-unsaturated ketones (chalcones). RAM achieves similar transformations to BM, though adjustments in reaction conditions may be necessary due to different mixing regimes.</p>","PeriodicalId":101140,"journal":{"name":"RSC Mechanochemistry","volume":" 3","pages":" 482-487"},"PeriodicalIF":0.0000,"publicationDate":"2025-03-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://pubs.rsc.org/en/content/articlepdf/2025/mr/d5mr00016e?page=search","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"RSC Mechanochemistry","FirstCategoryId":"1085","ListUrlMain":"https://pubs.rsc.org/en/content/articlelanding/2025/mr/d5mr00016e","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
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Abstract
By using in situ Raman spectroscopy for reaction monitoring, we compare ball milling (BM) and resonant acoustic mixing (RAM) in the preparation α,β-unsaturated ketones (chalcones). RAM achieves similar transformations to BM, though adjustments in reaction conditions may be necessary due to different mixing regimes.
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