Mrinal Dwivedi , Kannan Murugesan , N. Arunachalam , M.S. Ramachandra Rao
{"title":"Numerical simulation and validation of pressure transfer mechanism between anvil and pyrophyllite block in high pressure high temperature cubic press","authors":"Mrinal Dwivedi , Kannan Murugesan , N. Arunachalam , M.S. Ramachandra Rao","doi":"10.1016/j.diamond.2025.112332","DOIUrl":null,"url":null,"abstract":"<div><div>In High Pressure High Temperature (HPHT) cubic press, the pressure needs to be transmitted to the carbon metal catalyst system through different combination of material interfaces called the supercell. The supercell structure consists of the carbon metal catalyst system enclosed within a graphite heater surrounded by a thermal and electrical insulators. The pressure transmission to the pyrophyllite block which forms the outer envelope of the supercell is essential to ensure the pressure buildup inside the system. The understanding of this pressure transfer, however, is affected by the inability of using traditional monitoring methods due to extreme operating conditions. This requires use of Finite Element Method in order to gain in-depth understanding of the pressure transfer mechanism. In this work a novel finite element framework is used to analyze the pressure generation at the anvil pyrophyllite interface system and pressure transfer through the pyrophyllite. Modelling of Pyrophyllite requires use of Lagrangian elements which distort at high pressure conditions due to its elasto-plastic behavior. To overcome excessive element distortion, local re-meshing needs to be done which not only increases the computational effort but also leads to inaccurate results. This work proposes to use the Coupled Eulerian Lagrangian (CEL) technique to model anvil system where pyrophyllite is modelled using Eulerian elements and anvil is modelled using Lagrangian elements. This solves the issue of mesh distortion as Eulerian elements are fixed in space. Mohr-Columb criteria is used to capture the elasto-plastic behavior of the pyrophyllite. Pressure at the center of the pyrophyllite block is compared with experiments and an excellent match with error less than 1.6 % between the results is observed.</div></div>","PeriodicalId":11266,"journal":{"name":"Diamond and Related Materials","volume":"155 ","pages":"Article 112332"},"PeriodicalIF":4.3000,"publicationDate":"2025-04-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Diamond and Related Materials","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0925963525003899","RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, COATINGS & FILMS","Score":null,"Total":0}
引用次数: 0
Abstract
In High Pressure High Temperature (HPHT) cubic press, the pressure needs to be transmitted to the carbon metal catalyst system through different combination of material interfaces called the supercell. The supercell structure consists of the carbon metal catalyst system enclosed within a graphite heater surrounded by a thermal and electrical insulators. The pressure transmission to the pyrophyllite block which forms the outer envelope of the supercell is essential to ensure the pressure buildup inside the system. The understanding of this pressure transfer, however, is affected by the inability of using traditional monitoring methods due to extreme operating conditions. This requires use of Finite Element Method in order to gain in-depth understanding of the pressure transfer mechanism. In this work a novel finite element framework is used to analyze the pressure generation at the anvil pyrophyllite interface system and pressure transfer through the pyrophyllite. Modelling of Pyrophyllite requires use of Lagrangian elements which distort at high pressure conditions due to its elasto-plastic behavior. To overcome excessive element distortion, local re-meshing needs to be done which not only increases the computational effort but also leads to inaccurate results. This work proposes to use the Coupled Eulerian Lagrangian (CEL) technique to model anvil system where pyrophyllite is modelled using Eulerian elements and anvil is modelled using Lagrangian elements. This solves the issue of mesh distortion as Eulerian elements are fixed in space. Mohr-Columb criteria is used to capture the elasto-plastic behavior of the pyrophyllite. Pressure at the center of the pyrophyllite block is compared with experiments and an excellent match with error less than 1.6 % between the results is observed.
期刊介绍:
DRM is a leading international journal that publishes new fundamental and applied research on all forms of diamond, the integration of diamond with other advanced materials and development of technologies exploiting diamond. The synthesis, characterization and processing of single crystal diamond, polycrystalline films, nanodiamond powders and heterostructures with other advanced materials are encouraged topics for technical and review articles. In addition to diamond, the journal publishes manuscripts on the synthesis, characterization and application of other related materials including diamond-like carbons, carbon nanotubes, graphene, and boron and carbon nitrides. Articles are sought on the chemical functionalization of diamond and related materials as well as their use in electrochemistry, energy storage and conversion, chemical and biological sensing, imaging, thermal management, photonic and quantum applications, electron emission and electronic devices.
The International Conference on Diamond and Carbon Materials has evolved into the largest and most well attended forum in the field of diamond, providing a forum to showcase the latest results in the science and technology of diamond and other carbon materials such as carbon nanotubes, graphene, and diamond-like carbon. Run annually in association with Diamond and Related Materials the conference provides junior and established researchers the opportunity to exchange the latest results ranging from fundamental physical and chemical concepts to applied research focusing on the next generation carbon-based devices.