Effect of Surface Modification by Selective Oxidation on the Microstructure and Core Loss in Fe–3Si–5.5Cr Soft Magnetic Composite

IF 4.3 3区 材料科学 Q1 ENGINEERING, ELECTRICAL & ELECTRONIC
Sung-Min Park, Jae-Young Park, Chang-Soo Park, Kyung Rok Jang, Sun Dong Park, Dong Hoe Kim* and Hyung-Ki Park*, 
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Abstract

This study investigated the impact of selective oxidation on the core loss of soft magnetic composites. The Fe–3Si–5.5Cr powders were annealed in an atmosphere where Fe was reduced, and Cr and Si were selectively oxidized, forming an insulation oxide layer on the powder surface. To examine the core loss changes due to the insulation coating formed by selective oxidation, the toroidal core samples were fabricated using powders with and without selective oxidation. The core losses of the toroidal core samples fabricated by the selectively oxidized powders were reduced, and as the selective oxidation time increased, the core loss was further reduced. To analyze the cause of the reduction in core loss, the total core loss was separated into the hysteresis, eddy current, and anomalous losses based on the variable separation method. The three losses were reduced in the toroidal core samples fabricated by the selectively oxidized powder. These results confirmed that selective oxidation could form a uniform and dense insulation coating on the Fe–Si–Cr powder, effectively reducing the core loss.

Abstract Image

选择性氧化表面改性对Fe-3Si-5.5Cr软磁复合材料显微组织和磁芯损耗的影响
研究了选择性氧化对软磁复合材料磁芯损耗的影响。Fe - 3si - 5.5Cr粉末在Fe还原气氛中退火,Cr和Si选择性氧化,在粉末表面形成绝缘氧化层。为了研究选择性氧化形成的绝缘涂层对磁芯损耗的影响,分别用选择性氧化和不选择性氧化的粉末制备了环形磁芯样品。选择性氧化粉末制备的环形磁芯样品的磁芯损耗减小,并且随着选择性氧化时间的增加,磁芯损耗进一步减小。为了分析铁芯损耗降低的原因,采用变量分离法将铁芯总损耗分为磁滞、涡流和异常损耗。在选择性氧化粉末制备的环形芯样品中,这三种损耗都有所降低。这些结果证实了选择性氧化可以在Fe-Si-Cr粉末上形成均匀致密的绝缘涂层,有效地降低了铁芯损耗。
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来源期刊
CiteScore
7.20
自引率
4.30%
发文量
567
期刊介绍: ACS Applied Electronic Materials is an interdisciplinary journal publishing original research covering all aspects of electronic materials. The journal is devoted to reports of new and original experimental and theoretical research of an applied nature that integrate knowledge in the areas of materials science, engineering, optics, physics, and chemistry into important applications of electronic materials. Sample research topics that span the journal's scope are inorganic, organic, ionic and polymeric materials with properties that include conducting, semiconducting, superconducting, insulating, dielectric, magnetic, optoelectronic, piezoelectric, ferroelectric and thermoelectric. Indexed/​Abstracted: Web of Science SCIE Scopus CAS INSPEC Portico
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