Extraction of cellulose from bamboo (Bambusa vulgaris Schrad. ex J.C. Wendl.) for bio-foam applications

Norhafizah Saari , Sitti Fatimah Mhd Ramle , Nur Salsabilla Zahidan , Nur Ayuni Ahmad , Zubaidah Aimi Abdul Hamid , Abdul Fattah Nongman , Nurul Fazita Mohamad Rawi
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Abstract

Cellulose bio-foam (CBF) was developed using bamboo (Bambusa vulgaris Schrad. ex J.C. Wendl.) cellulose with varying fibre content concentrations (0 %, 10 % and 20 %) incorporated with starch and glycerol through the evaporative drying method. The morphology and microstructure of the CBF were analysed using scanning electron microscopy and optical light microscopy. Results revealed that CBF with 0 % cellulose fibre content exhibited a smoother surface compared to the rougher textures observed in 10 % and 20 % fibre content. The addition of cellulose fibres increased both the average and mean cell sizes, with pore sizes ranging from 0.93 mm to 2.69 mm for 10 % and from 0.94 mm to 3.27 mm for 20 %. Energy-dispersive X-ray (EDX) analysis confirmed the presence of cellulose microfibrils through the detection of carbon and oxygen elements. Thermogravimetric analysis further demonstrated that the accumulation of glycerol on the surface of microfibrils at 20 % cellulose fibre content enhanced the thermal stability of the CBF by increasing its degradation temperature. Notably, the addition of cellulose fibres significantly improved the mechanical properties of the CBF. Among the samples, CBF with 10 % cellulose content exhibited the highest mechanical strength, with a Young’s modulus of 78.74 N/m², compared to 6.91 N/m² for 0 % and 59.71 N/m² for 20 %. These findings highlight the optimal performance of CBF with 10 % cellulose content in terms of mechanical strength and overall material properties.
竹材纤维素的提取研究。如J.C.温德尔)的生物泡沫应用
以竹材为原料制备纤维素生物泡沫(CBF)。(ex J.C. Wendl.)不同纤维含量浓度(0 %,10 %和20 %)的纤维素,通过蒸发干燥法掺入淀粉和甘油。利用扫描电子显微镜和光学显微镜对CBF的形貌和微观结构进行了分析。结果表明,与纤维含量为10 %和20 %的CBF相比,0 %纤维素纤维含量的CBF表面更光滑。纤维素纤维的加入增加了平均和平均细胞尺寸,孔径范围从0.93 mm到2.69 mm(占10% %),从0.94 mm到3.27 mm(占20% %)。能量色散x射线(EDX)分析通过检测碳和氧元素证实了纤维素微原纤维的存在。热重分析进一步表明,当纤维素纤维含量为20% %时,甘油在微纤维表面的积累通过提高其降解温度来增强CBF的热稳定性。值得注意的是,纤维素纤维的加入显著改善了CBF的机械性能。其中,纤维素含量为10 %的CBF的机械强度最高,杨氏模量为78.74 N/m²,而纤维素含量为0 %和20 %的CBF的杨氏模量分别为6.91 N/m²和59.71 N/m²。这些发现突出了纤维素含量为10 %的CBF在机械强度和整体材料性能方面的最佳性能。
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