Synthesis of 1-[3-(trimethoxysilyl)propyl]-1H-1,2,4-triazole

IF 1.7 4区 化学 Q3 CHEMISTRY, MULTIDISCIPLINARY
N. A. El’kov, Dzh. N. Konshina, I. A. Lupanova, E. S. Spesivaya, V. V. Konshin
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引用次数: 0

Abstract

By alkylation of the sodium salt of 1,2,4-triazole with (3-chloropropyl)trimethoxysilane in a boiling toluene—DMF mixture for 3 h, 1-[3-(trimethoxysifyl)propyl]-1H-1,2,4-triazole was synthesized with a yield of 86%. The possibility of the use of this compound to obtain materials with covalently immobilized 1,2,4-triazole moieties both by modifying the surface of silica gel and by the sol—gel process using joint hydrolytic condensation with tetraethoxysilane was shown.

1-[3-(三甲氧基硅基)丙基]-1H-1,2,4-三唑的合成
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来源期刊
Russian Chemical Bulletin
Russian Chemical Bulletin 化学-化学综合
CiteScore
2.70
自引率
47.10%
发文量
257
审稿时长
3-8 weeks
期刊介绍: Publishing nearly 500 original articles a year, by leading Scientists from Russia and throughout the world, Russian Chemical Bulletin is a prominent international journal. The coverage of the journal spans practically all areas of fundamental chemical research and is presented in five sections: General and Inorganic Chemistry; Physical Chemistry; Organic Chemistry; Organometallic Chemistry; Chemistry of Natural Compounds and Bioorganic Chemistry.
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