Effects of Sn on microstructure and tensile properties in a binary Mg-1Ca alloy

M.B. Mesbah , H.M.M.A. Rashed
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Abstract

The evolution of microstructure and tensile properties of a binary Mg-1Ca alloy with different tin additions (1, 2, and 4 wt%) was investigated under various conditions of temperatures and strain rates. Mg-1Ca, Mg-1Ca-1Sn, Mg-1Ca-2Sn, and Mg-1Ca-4Sn samples were cast and homogenized. The homogenized samples were rolled at 400 °C. Optical microstructures of both cast and rolled samples were taken for microstructural analysis. Scanning electron microscopy of four rolled samples was carried out to identify the phases present. Tensile test of rolled alloys was carried out at temperatures 300, 350, 400, and 450 °C, and at two different strain rates 5x 104 s1 and 1x 104 s1. It was found that tin addition increased dendrite formation in as-cast alloys and continuously reduced the grain sizes of rolled alloys. The addition of a small amount of Sn increased both strength and elongation to failure values. However, a higher amount of Sn addition lowered the properties to some extent due to the formation of excessive intermetallic particles. At lower temperatures, higher strength and lower elongation to failure values were found due to higher work hardening. Conversely, at elevated temperatures, strength values were reduced due to inevitable softening and greater grain growth.
Sn对Mg-1Ca二元合金组织和拉伸性能的影响
研究了不同锡添加量(1、2和4 wt%)下Mg-1Ca二元合金在不同温度和应变速率下的组织和拉伸性能演变。对Mg-1Ca、Mg-1Ca- 1sn、Mg-1Ca- 2sn和Mg-1Ca- 4sn样品进行铸造和均匀化处理。均质后的样品在400℃下轧制。采用光学显微组织对铸轧试样进行显微组织分析。用扫描电子显微镜对四个轧制样品进行了相鉴定。轧制合金在300、350、400和450℃的温度下,以5 × 10−4 s−1和1 × 10−4 s−1两种不同的应变速率进行拉伸试验。结果表明,锡的加入增加了铸态合金枝晶的形成,并使轧制合金的晶粒尺寸不断减小。少量Sn的加入使强度和伸长率均达到破坏值。然而,由于过量的金属间颗粒的形成,较高的Sn添加量在一定程度上降低了性能。在较低的温度下,由于较高的加工硬化,发现较高的强度和较低的延伸率。相反,在高温下,由于不可避免的软化和更大的晶粒生长,强度值降低。
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CiteScore
5.30
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