{"title":"Influence of bulk post processing techniques on anisotropy of microstructural and tribological properties of L-DED produced Ti64 alloy","authors":"Sanju Suresh , Jino Joshy , Basil Kuriachen , Ravi Chandan Gurugubelli , Vikash Kumar , Srikanth Bontha","doi":"10.1016/j.wear.2025.206014","DOIUrl":null,"url":null,"abstract":"<div><div>Laser-Direct Energy Deposited (L-DED) Ti64 alloy is known to have high anisotropy, and low wear resistance which reduce the longevity of artificial bone joints. Thus, the primary objective of this study is to compare and contrast the effect of bulk treatments to mitigate these inherent limitations. Keeping printing parameters constant, the printed samples were put through different post-treatments, namely, super-β annealing (1050 °C, 1 h) and deep cryogenic dipping (−196 °C, 48 h). Electron back scatter diffraction (EBSD) and x-ray diffraction (XRD) analysis revealed differences in grain morphology and phase distributions in the treated samples. A linear reciprocating wear test is conducted with Al<sub>2</sub>O<sub>3</sub> as the counter body to mimic the artificial hip socket. The super-β annealing process reduced the anisotropy in wear rate from 76 % to 60 % but did not show an overall betterment. On the other hand, the cryo-treatment showed an 83 % reduction in wear and a slight reduction in anisotropy compared to the as-build sample. The coefficient of friction (COF) plots also displayed an increase for annealed samples (15.4%–31.5 % higher) while showing a major reduction in cryo-treated samples (42.8%–54.7 % reduction).</div></div>","PeriodicalId":23970,"journal":{"name":"Wear","volume":"572 ","pages":"Article 206014"},"PeriodicalIF":5.3000,"publicationDate":"2025-03-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Wear","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0043164825002832","RegionNum":1,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"ENGINEERING, MECHANICAL","Score":null,"Total":0}
引用次数: 0
Abstract
Laser-Direct Energy Deposited (L-DED) Ti64 alloy is known to have high anisotropy, and low wear resistance which reduce the longevity of artificial bone joints. Thus, the primary objective of this study is to compare and contrast the effect of bulk treatments to mitigate these inherent limitations. Keeping printing parameters constant, the printed samples were put through different post-treatments, namely, super-β annealing (1050 °C, 1 h) and deep cryogenic dipping (−196 °C, 48 h). Electron back scatter diffraction (EBSD) and x-ray diffraction (XRD) analysis revealed differences in grain morphology and phase distributions in the treated samples. A linear reciprocating wear test is conducted with Al2O3 as the counter body to mimic the artificial hip socket. The super-β annealing process reduced the anisotropy in wear rate from 76 % to 60 % but did not show an overall betterment. On the other hand, the cryo-treatment showed an 83 % reduction in wear and a slight reduction in anisotropy compared to the as-build sample. The coefficient of friction (COF) plots also displayed an increase for annealed samples (15.4%–31.5 % higher) while showing a major reduction in cryo-treated samples (42.8%–54.7 % reduction).
期刊介绍:
Wear journal is dedicated to the advancement of basic and applied knowledge concerning the nature of wear of materials. Broadly, topics of interest range from development of fundamental understanding of the mechanisms of wear to innovative solutions to practical engineering problems. Authors of experimental studies are expected to comment on the repeatability of the data, and whenever possible, conduct multiple measurements under similar testing conditions. Further, Wear embraces the highest standards of professional ethics, and the detection of matching content, either in written or graphical form, from other publications by the current authors or by others, may result in rejection.