Electrochemical Study of Selective Laser Melted Inconel 718 Alloy Subjected to Varying Aging Durations

IF 2.1 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
JOM Pub Date : 2024-12-16 DOI:10.1007/s11837-024-07032-0
Abdelgadir M. Abdelgadir, Murtaza Siddiqui, Akeem Y. Adesina, Syed Sohail Akhtar
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Abstract

In this study, heat treatment with varying aging durations is applied on specimens produced by selective laser melting of pre-alloyed powder of Inconel 718 alloy (IN718) to evaluate the impact of aging duration on the microstructure and corrosion resistance. A two-stage aging procedure was adopted after homogenizing the samples at 1000°C for 1 h. The aging was initially done at 740°C for 8 h then cooled to 620°C and kept for 8 h, 15 h, 25 h, and 40 h in the second stage before finally being normalized under ambient conditions. The results revealed that corrosion resistance improved significantly with longer aging durations, with the 40-h aged sample exhibiting the highest resistance. The enhanced corrosion resistance is attributed to the precipitation of γ′ and γ″ phases. Pitting corrosion resistance increased with aging duration up to 15 h in the second stage, then slightly decreased because of overaging. Similarly, hardness declined slightly beyond 25 h of aging because of the transformation of γ′ and γ″ phases into the δ phase. This study emphasizes the need for precise control of aging durations to optimize corrosion resistance and mechanical properties.

Abstract Image

在本研究中,对通过选择性激光熔化 Inconel 718 合金(IN718)预合金化粉末生产的试样进行了不同老化持续时间的热处理,以评估老化持续时间对微观结构和耐腐蚀性的影响。样品在 1000°C 下均质 1 小时后,采用了两阶段时效程序。初始时效在 740°C 下进行 8 小时,然后冷却至 620°C,在第二阶段分别保持 8 小时、15 小时、25 小时和 40 小时,最后在环境条件下进行正火。结果表明,随着老化时间的延长,耐腐蚀性显著提高,老化 40 小时的样品耐腐蚀性最高。耐腐蚀性的增强归因于γ′和γ″相的析出。耐点蚀性随着时效时间的延长而增加,第二阶段达到 15 小时,然后由于时效过长而略有下降。同样,由于γ′和γ″相转变为δ相,硬度在时效超过 25 小时后略有下降。这项研究强调了精确控制老化持续时间以优化耐腐蚀性和机械性能的必要性。
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来源期刊
JOM
JOM 工程技术-材料科学:综合
CiteScore
4.50
自引率
3.80%
发文量
540
审稿时长
2.8 months
期刊介绍: JOM is a technical journal devoted to exploring the many aspects of materials science and engineering. JOM reports scholarly work that explores the state-of-the-art processing, fabrication, design, and application of metals, ceramics, plastics, composites, and other materials. In pursuing this goal, JOM strives to balance the interests of the laboratory and the marketplace by reporting academic, industrial, and government-sponsored work from around the world.
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