Joo Hyeong Suh, Sang A Han, Soo Young Yang, Jun Won Lee, Yusuke Shimada, Sang-Min Lee, Jong-Won Lee, Min-Sik Park, Jung Ho Kim
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引用次数: 0
Abstract
Adv. Mater. 2025, 37, 2414117
DOI: 10.1002/adma.202414117
We noted that some essential details required for reproducibility—such as the raw materials used, detailed synthetic procedures, and specific time and temperature conditions—were omitted. To address this, we have added a “Materials Synthesis” section, provided below:
Materials Synthesis
To prepare MoS2-NG, 0.2 g of molybdenum oxide (MoO3, purity >99.9%, Sigma–Aldrich) powder was dispersed in 30 mL of hydrogen peroxide (H2O2, 35%, Sigma–Aldrich) under continuous stirring at 300 rpm for 24 h at 80 °C, forming a-MoOx-NG. The as-prepared 2.5 g of a-MoOx-NG was then calcined at 600 °C for 6 h in a vertical furnace under argon (Ar) gas flow to obtain c-MoOx-NG. Next, 0.4 g of thiourea (CH4N2S, purity >99.0%, Sigma–Aldrich) and the obtained powder were dispersed in 100 mL of deionized (DI) water inside a Teflon-lined stainless-steel autoclave. A hydrothermal treatment was conducted at 200 °C for 24 h, followed by cooling to room temperature. The final product was collected via centrifugation at 8000 rpm for 10 min, repeated five times using a mixture (5:5 v/v) of DI water and ethanol (CH3CH2OH, 99.5%, Sigma–Aldrich). Finally, the MoS2-NG was dried in a convection oven at 80 °C for 12 h.
期刊介绍:
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