S. A. Tuychiev, U. A. Madatov, A. S. Togasharov, B. S. Zakirov
{"title":"Solubility in System Sodium Chlorate Monocarbamide–Acetamide–Water","authors":"S. A. Tuychiev, U. A. Madatov, A. S. Togasharov, B. S. Zakirov","doi":"10.1134/S0036023624601995","DOIUrl":null,"url":null,"abstract":"<p>The solubility of the substances in the NaClO<sub>3</sub>∙CO(NH<sub>2</sub>)<sub>2</sub>–C<sub>2</sub>H<sub>5</sub>NO–H<sub>2</sub>O system was examined using a visual-polythermal method in the temperature range from –39.0 to 78.0°С. A solubility diagram was created based on the results. In the phase diagram of the system, the crystallization fields of ice, CO(NH<sub>2</sub>)<sub>2</sub>, NaClO<sub>3</sub>, and C<sub>2</sub>H<sub>5</sub>NO, as well as a new compound NaClO<sub>3</sub>∙CO(NH<sub>2</sub>)<sub>2</sub>∙C<sub>2</sub>H<sub>5</sub>NO, were separated. The compound was successfully isolated and confirmed to be novel based on the results of physicochemical analysis.</p>","PeriodicalId":762,"journal":{"name":"Russian Journal of Inorganic Chemistry","volume":"69 14","pages":"2131 - 2139"},"PeriodicalIF":1.8000,"publicationDate":"2024-12-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Russian Journal of Inorganic Chemistry","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1134/S0036023624601995","RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"CHEMISTRY, INORGANIC & NUCLEAR","Score":null,"Total":0}
引用次数: 0
Abstract
The solubility of the substances in the NaClO3∙CO(NH2)2–C2H5NO–H2O system was examined using a visual-polythermal method in the temperature range from –39.0 to 78.0°С. A solubility diagram was created based on the results. In the phase diagram of the system, the crystallization fields of ice, CO(NH2)2, NaClO3, and C2H5NO, as well as a new compound NaClO3∙CO(NH2)2∙C2H5NO, were separated. The compound was successfully isolated and confirmed to be novel based on the results of physicochemical analysis.
期刊介绍:
Russian Journal of Inorganic Chemistry is a monthly periodical that covers the following topics of research: the synthesis and properties of inorganic compounds, coordination compounds, physicochemical analysis of inorganic systems, theoretical inorganic chemistry, physical methods of investigation, chemistry of solutions, inorganic materials, and nanomaterials.