S. V. Saikova, E. A. Kirshneva, N. P. Fadeeva, O. A. Bayukov, Yu. V. Knyazev, M. N. Volochaev, A. S. Samoilo
{"title":"Influence of Heat Treatment Conditions on the Production of Ultrafine Erbium Iron Garnet Powders Using Anion Exchange Resin Assisted Precipitation","authors":"S. V. Saikova, E. A. Kirshneva, N. P. Fadeeva, O. A. Bayukov, Yu. V. Knyazev, M. N. Volochaev, A. S. Samoilo","doi":"10.1134/S0036023624601673","DOIUrl":null,"url":null,"abstract":"<p>This work proposes a method for the preparation of nanostructured Er<sub>3</sub>Fe<sub>5</sub>O<sub>12</sub> powders, comprising the anion-exchange resin assisted coprecipitation of erbium and iron(III) ions and subsequent heat treatment of the products. Optimal conditions for the anion-exchange precipitation of a highly reactive stoichiometric precursor were determined, and the influence of the heat-treatment schedule on the yield and stability of erbium ferrite garnet nanoparticles was investigated. The prepared nanomaterials were characterized by X-ray powder diffraction analysis, electron microscopy, thermal analysis, and Mössbauer spectroscopy. This synthesis method provides iron-erbium garnet with an average particle size of 25 nm at 800°C. The discovered patterns can be used to develop new methods for the synthesis of rare-earth garnet compounds.</p>","PeriodicalId":762,"journal":{"name":"Russian Journal of Inorganic Chemistry","volume":"69 12","pages":"1789 - 1797"},"PeriodicalIF":1.8000,"publicationDate":"2024-12-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Russian Journal of Inorganic Chemistry","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1134/S0036023624601673","RegionNum":3,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"CHEMISTRY, INORGANIC & NUCLEAR","Score":null,"Total":0}
引用次数: 0
Abstract
This work proposes a method for the preparation of nanostructured Er3Fe5O12 powders, comprising the anion-exchange resin assisted coprecipitation of erbium and iron(III) ions and subsequent heat treatment of the products. Optimal conditions for the anion-exchange precipitation of a highly reactive stoichiometric precursor were determined, and the influence of the heat-treatment schedule on the yield and stability of erbium ferrite garnet nanoparticles was investigated. The prepared nanomaterials were characterized by X-ray powder diffraction analysis, electron microscopy, thermal analysis, and Mössbauer spectroscopy. This synthesis method provides iron-erbium garnet with an average particle size of 25 nm at 800°C. The discovered patterns can be used to develop new methods for the synthesis of rare-earth garnet compounds.
期刊介绍：
Russian Journal of Inorganic Chemistry is a monthly periodical that covers the following topics of research: the synthesis and properties of inorganic compounds, coordination compounds, physicochemical analysis of inorganic systems, theoretical inorganic chemistry, physical methods of investigation, chemistry of solutions, inorganic materials, and nanomaterials.
求助内容：
应助结果提醒方式：
京公网安备 11010802042870号
