Effect of Heat Input on the Microstructure and Phase Composition of Additively Manufactured Ti–6Al–4V Alloy

IF 0.5 Q4 PHYSICS, CONDENSED MATTER
K. D. Kamelina, A. V. Panin, M. S. Syrtanov
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引用次数: 0

Abstract

Optical microscopy and X-ray phase analysis are used to investigate the grain structure and phase composition of Ti–6Al–4V titanium-alloy samples produced by wire-feed electron beam additive manufacturing using a linear strategy. X-ray fluorescence analysis is employed to examine the elemental composition of the Ti–6Al–4V alloy samples fabricated through 3D printing. The samples are rectangular plates cut from bars, which are produced under varying thermal-exposure parameters, specifically different beam currents and 3D-printing speeds. We compare the elemental composition of the printed Ti–6Al–4V samples with that of the wire from which they were produced. The effect of heat-input magnitude on the sizes of primary β‑phase grains and α-phase plates in the samples and the volumetric fraction of the residual β phase is determined. We demonstrate how the sizes of primary β-phase grains and α-phase plates, along with the volumetric fraction of the residual β-phase, change with increasing distance from the contact point of the samples with the substrate. We propose hypotheses regarding the causes of these changes. The effect of the substrate on the elemental and phase composition of the samples is also shown.

Abstract Image

热输入对增材制造Ti-6Al-4V合金组织和相组成的影响
采用光学显微镜和x射线相分析方法研究了线馈电子束增材制造Ti-6Al-4V钛合金样品的晶粒结构和相组成。采用x射线荧光分析技术对3D打印制备的Ti-6Al-4V合金样品进行元素组成分析。样品是从棒材上切下来的矩形板,在不同的热暴露参数下生产,特别是不同的光束电流和3d打印速度。我们比较了印刷Ti-6Al-4V样品的元素组成与生产它们的金属丝的元素组成。测定了热输入量级对试样中初生β相晶粒和α相板尺寸及残余β相体积分数的影响。我们展示了初生β相晶粒和α相板的尺寸,以及剩余β相的体积分数是如何随着样品与底物接触点距离的增加而变化的。我们对这些变化的原因提出了假设。实验还显示了衬底对样品元素组成和相组成的影响。
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来源期刊
CiteScore
0.90
自引率
25.00%
发文量
144
审稿时长
3-8 weeks
期刊介绍: Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques publishes original articles on the topical problems of solid-state physics, materials science, experimental techniques, condensed media, nanostructures, surfaces of thin films, and phase boundaries: geometric and energetical structures of surfaces, the methods of computer simulations; physical and chemical properties and their changes upon radiation and other treatments; the methods of studies of films and surface layers of crystals (XRD, XPS, synchrotron radiation, neutron and electron diffraction, electron microscopic, scanning tunneling microscopic, atomic force microscopic studies, and other methods that provide data on the surfaces and thin films). Articles related to the methods and technics of structure studies are the focus of the journal. The journal accepts manuscripts of regular articles and reviews in English or Russian language from authors of all countries. All manuscripts are peer-reviewed.
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