Resin composite color change by spatula manipulation, effects on surface and color stability.

Samara R Dos Santos Franco, Jorge E da Silva Junior, Waldemir F Vieira Junior, Fabiana Mantovani Gomes França, Cecilia Pedroso Turssi, Roberta Tarkany Basting
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引用次数: 0

Abstract

Aim: To evaluate the influence of spatulas on resin composite color stability, and characterize the surface of both the spatulas and the resin composites before and after manipulation.

Materials and method: Discs (ø6 mm x 2 mm) of suprananofilled resin composite (Palfique LX5/Tokuyama) and nanohybrid resin (Empress Direct/Ivoclar Vivadent) were fabricated. They were divided into groups (n=10), and manipulated with different spatulas: non-manipulated (control), metal spatulas (Almore Millennium/ Golgran, Almore #3/ Quinelato, LM Arte Modella/ Quinelato), or plastic spatulas (Jon). Manipulation involved lightly pressing the spatula 50 times against the resin composite on waterproof paper. Color was analyzed at three time points: immediately, after finishing and polishing, and after 24-hour immersion in distilled water, with CIELab* parameters, ΔEab, ΔE00, and ΔWID. Spatulas and resins were submitted to micromorphological and energy-dispersive X-ray spectroscopic (EDS) analysis. Generalized linear models or Kruskal-Wallis and Dunn tests (α=5%) were applied.

Results: Resin color changed after manipulation with a metal spatula, but there was no significant difference in ΔEab and ΔE00 for the resin composites according to the spatula (p>0.05). The suprananofilled resin varied more than the nanohybrid resin over time (p<0.05). Abrasive wear was observed on the spatulas after manipulating the resin composites, with greater wear for the spatulas used with suprananofilled resin. EDS showed different spatula and resin composite compositions.

Conclusions: Metal spatulas influenced resin composite color stability, with greater color change for suprananofilled resin. The spatulas exhibited abrasive wear, attributable to the difference in hardness between the spatulas and the resin composites.

目的:评估抹刀对树脂复合材料颜色稳定性的影响,并描述抹刀和树脂复合材料在操作前和操作后的表面特征:制作超填料树脂复合材料(Palfique LX5/Tokuyama)和纳米杂化树脂(Empress Direct/Ivoclar Vivadent)的圆盘(ø6 mm x 2 mm)。将它们分成几组(n=10),用不同的刮铲进行操作:无操作(对照组)、金属刮铲(Almore Millennium/ Golgran、Almore #3/Quinelato、LM Arte Modella/ Quinelato)或塑料刮铲(Jon)。操作方法是用刮刀轻轻按压防水纸上的树脂复合材料 50 次。在三个时间点对颜色进行了分析:即刻、精加工和抛光后以及在蒸馏水中浸泡 24 小时后,使用 CIELab* 参数ΔEab、ΔE00 和 ΔWID。对抹刀和树脂进行了微观形态和能量色散 X 射线光谱(EDS)分析。应用广义线性模型或 Kruskal-Wallis 和 Dunn 检验(α=5%):用金属刮刀操作后,树脂的颜色发生了变化,但根据刮刀的不同,树脂复合材料的 ΔEab 和 ΔE00 没有显著差异(p>0.05)。随着时间的推移,超填料树脂比纳米杂化树脂的变化更大(p 结论:金属刮刀影响树脂复合材料的颜色稳定性,超填料树脂的颜色变化更大。金属刮刀出现磨损,这是由于刮刀和树脂复合材料的硬度不同造成的。
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