Chemical method of doping Inconel 713C powder with rhenium for 3D printed manufacturing. Influence of rhenium dopants on the microstructure changes

IF 4.4 3区 工程技术 Q1 ENGINEERING, CIVIL
Iwona Cieślik, Holger Seidlitz, Monika Duchna, Dariusz Zasada, Mirosław Kwaśny, Bogusława Adamczyk-Cieślak
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引用次数: 0

Abstract

A well-known method of doping powders in the industry is mechanical alloying synthesis. This method synthesizes metal powders by grinding them in high-energy mills, which prevents the achievement of well-dispersed particles throughout the volume and control of particle morphology, size, and agglomeration.

In the present work, rhenium doping of IN 713C was carried out in a polyester network system based on organic acids and diols with specially selected catalysts and experimental parameters leading to the complexation of Rhenium ions. In addition, neutral reagents were used in this research, contributing to the greening of many key industries. The obtained IN 713C powder with rhenium showed high dispersion without agglomeration effect and reasonable flowability. Depending on the polymerization process parameters, the morphology of the rhenium particles on the surface of IN 713C can be modified. The IN 713C powder, with and without rhenium, was used in the SLM process to fabricate IN 713C alloy samples. The study examines the effect of rhenium doped IN 713C on the microstructure and hardness changes of the alloy produced by the 3D-printing methods. This type of chemical modification methods can effectively enhance the hardness and affects the elongation of dendrites in the structure of IN 713C alloys manufactured by the additive methods.

Abstract Image

用铼掺杂铬镍铁合金713C粉末制造3D打印的化学方法。铼掺杂对微观结构变化的影响
工业上比较有名的掺杂粉末的方法是机械合金化合成。这种方法通过在高能研磨机中研磨金属粉末来合成金属粉末,这阻碍了颗粒在整个体积和颗粒形态、大小和团聚的控制中得到良好分散。在本研究中,采用特殊的催化剂和实验参数,在以有机酸和二醇为基础的聚酯网络体系中,对In 713C进行了铼掺杂,使铼离子络合。此外,本研究还使用了中性试剂,为许多重点行业的绿色化做出了贡献。制备的含铼IN 713C粉体分散性好,无团聚效应,流动性合理。根据聚合工艺参数的不同,可以改变IN 713C表面铼颗粒的形态。采用含铼和不含铼的IN 713C粉末在SLM工艺中制备了IN 713C合金样品。研究了掺铼的IN 713C对3d打印合金显微组织和硬度变化的影响。这类化学改性方法可以有效提高添加剂法制备的in 713C合金的硬度,并影响其组织中枝晶的延伸率。
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来源期刊
Archives of Civil and Mechanical Engineering
Archives of Civil and Mechanical Engineering 工程技术-材料科学:综合
CiteScore
6.80
自引率
9.10%
发文量
201
审稿时长
4 months
期刊介绍: Archives of Civil and Mechanical Engineering (ACME) publishes both theoretical and experimental original research articles which explore or exploit new ideas and techniques in three main areas: structural engineering, mechanics of materials and materials science. The aim of the journal is to advance science related to structural engineering focusing on structures, machines and mechanical systems. The journal also promotes advancement in the area of mechanics of materials, by publishing most recent findings in elasticity, plasticity, rheology, fatigue and fracture mechanics. The third area the journal is concentrating on is materials science, with emphasis on metals, composites, etc., their structures and properties as well as methods of evaluation. In addition to research papers, the Editorial Board welcomes state-of-the-art reviews on specialized topics. All such articles have to be sent to the Editor-in-Chief before submission for pre-submission review process. Only articles approved by the Editor-in-Chief in pre-submission process can be submitted to the journal for further processing. Approval in pre-submission stage doesn''t guarantee acceptance for publication as all papers are subject to a regular referee procedure.
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