{"title":"Effects of Yb element on microstructure and mechanical properties of high-strength Mg-Sm-Gd(-Yb)-Zr extruded alloys","authors":"Nana Zhang, Xiaoya Chen, Quanan Li, Zeyu Zheng, Zheng Wu, Jiaqi Xie","doi":"10.1016/j.jma.2025.02.006","DOIUrl":null,"url":null,"abstract":"A high-strength magnesium alloy containing Yb was prepared through a simple hot extrusion process. The effect of Yb addition on dynamic precipitation, texture evolution, dynamic recrystallization mechanisms, deformation mechanisms, and strengthening mechanisms in as-extruded Mg-4Sm-3Gd(-2Yb)-0.5Zr (SGY0, SGY2) alloys was systematically investigated. The results indicated that the average grain size decreased from 4.17 µm to 1.48 µm with the addition of Yb. This extreme grain refinement greatly enhances the strength. The addition of Yb significantly facilitated the phase precipitation, but did not change the texture type. The non-dynamic recrystallized (unDRXed) grains exhibited a strong basal plane texture of <01<span><span style=\"\"><math><mover accent=\"true\" is=\"true\"><mn is=\"true\">1</mn><mo is=\"true\">¯</mo></mover></math></span><span style=\"font-size: 90%; display: inline-block;\" tabindex=\"0\"><svg focusable=\"false\" height=\"2.202ex\" role=\"img\" style=\"vertical-align: -0.235ex;\" viewbox=\"0 -846.5 570.5 947.9\" width=\"1.325ex\" xmlns:xlink=\"http://www.w3.org/1999/xlink\"><g fill=\"currentColor\" stroke=\"currentColor\" stroke-width=\"0\" transform=\"matrix(1 0 0 -1 0 0)\"><g is=\"true\"><g is=\"true\" transform=\"translate(35,0)\"><use xlink:href=\"#MJMAIN-31\"></use></g><g is=\"true\" transform=\"translate(0,198)\"><use x=\"-70\" xlink:href=\"#MJMAIN-AF\" y=\"0\"></use><use x=\"70\" xlink:href=\"#MJMAIN-AF\" y=\"0\"></use></g></g></g></svg></span><script type=\"math/mml\"><math><mover accent=\"true\" is=\"true\"><mn is=\"true\">1</mn><mo is=\"true\">¯</mo></mover></math></script></span>0> parallel to the extrusion direction (ED), while the dynamic recrystallized (DRXed) grains showed a weaker rare earth texture, characterized by <<span><span style=\"\"><math><mrow is=\"true\"><mover is=\"true\"><mrow is=\"true\"><mn is=\"true\">1</mn></mrow><mo is=\"true\" stretchy=\"true\">‾</mo></mover><mn is=\"true\">2</mn><mover is=\"true\"><mrow is=\"true\"><mn is=\"true\">1</mn></mrow><mo is=\"true\" stretchy=\"true\">‾</mo></mover><mn is=\"true\">2</mn></mrow></math></span><span style=\"font-size: 90%; display: inline-block;\" tabindex=\"0\"><svg focusable=\"false\" height=\"2.202ex\" role=\"img\" style=\"vertical-align: -0.235ex;\" viewbox=\"0 -846.5 2142 947.9\" width=\"4.975ex\" xmlns:xlink=\"http://www.w3.org/1999/xlink\"><g fill=\"currentColor\" stroke=\"currentColor\" stroke-width=\"0\" transform=\"matrix(1 0 0 -1 0 0)\"><g is=\"true\"><g is=\"true\"><g is=\"true\" transform=\"translate(35,0)\"><g is=\"true\"><use xlink:href=\"#MJMAIN-31\"></use></g></g><g is=\"true\" transform=\"translate(0,198)\"><use x=\"-70\" xlink:href=\"#MJMAIN-AF\" y=\"0\"></use><use x=\"70\" xlink:href=\"#MJMAIN-AF\" y=\"0\"></use></g></g><g is=\"true\" transform=\"translate(570,0)\"><use xlink:href=\"#MJMAIN-32\"></use></g><g is=\"true\" transform=\"translate(1071,0)\"><g is=\"true\" transform=\"translate(35,0)\"><g is=\"true\"><use xlink:href=\"#MJMAIN-31\"></use></g></g><g is=\"true\" transform=\"translate(0,198)\"><use x=\"-70\" xlink:href=\"#MJMAIN-AF\" y=\"0\"></use><use x=\"70\" xlink:href=\"#MJMAIN-AF\" y=\"0\"></use></g></g><g is=\"true\" transform=\"translate(1641,0)\"><use xlink:href=\"#MJMAIN-32\"></use></g></g></g></svg></span><script type=\"math/mml\"><math><mrow is=\"true\"><mover is=\"true\"><mrow is=\"true\"><mn is=\"true\">1</mn></mrow><mo stretchy=\"true\" is=\"true\">‾</mo></mover><mn is=\"true\">2</mn><mover is=\"true\"><mrow is=\"true\"><mn is=\"true\">1</mn></mrow><mo stretchy=\"true\" is=\"true\">‾</mo></mover><mn is=\"true\">2</mn></mrow></math></script></span>> // ED. Moreover, the as-extruded SGY0 and SGY2 alloys predominantly undergo continuous dynamic recrystallization (CDRX), and some DRXed grains exhibit a discontinuous dynamic recrystallization mechanism (DDRX). In addition, the addition of Yb facilitates the activation of non-basal plane slip. The dislocation types in the as-extruded SGY0 and SGY2 alloys include 〈a〉, 〈c〉 and 〈<em>c</em> + <em>a</em>〉 dislocations. However, the SGY2 alloy exhibits a relatively high dislocation density, which contributes to the enhancement of the strength. Extreme grain refinement and the dispersion of nanoscale second-phase particles are key factors in increasing the strength.","PeriodicalId":16214,"journal":{"name":"Journal of Magnesium and Alloys","volume":"185 1","pages":""},"PeriodicalIF":15.8000,"publicationDate":"2025-02-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Magnesium and Alloys","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1016/j.jma.2025.02.006","RegionNum":1,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"METALLURGY & METALLURGICAL ENGINEERING","Score":null,"Total":0}
引用次数: 0
Abstract
A high-strength magnesium alloy containing Yb was prepared through a simple hot extrusion process. The effect of Yb addition on dynamic precipitation, texture evolution, dynamic recrystallization mechanisms, deformation mechanisms, and strengthening mechanisms in as-extruded Mg-4Sm-3Gd(-2Yb)-0.5Zr (SGY0, SGY2) alloys was systematically investigated. The results indicated that the average grain size decreased from 4.17 µm to 1.48 µm with the addition of Yb. This extreme grain refinement greatly enhances the strength. The addition of Yb significantly facilitated the phase precipitation, but did not change the texture type. The non-dynamic recrystallized (unDRXed) grains exhibited a strong basal plane texture of <010> parallel to the extrusion direction (ED), while the dynamic recrystallized (DRXed) grains showed a weaker rare earth texture, characterized by <> // ED. Moreover, the as-extruded SGY0 and SGY2 alloys predominantly undergo continuous dynamic recrystallization (CDRX), and some DRXed grains exhibit a discontinuous dynamic recrystallization mechanism (DDRX). In addition, the addition of Yb facilitates the activation of non-basal plane slip. The dislocation types in the as-extruded SGY0 and SGY2 alloys include 〈a〉, 〈c〉 and 〈c + a〉 dislocations. However, the SGY2 alloy exhibits a relatively high dislocation density, which contributes to the enhancement of the strength. Extreme grain refinement and the dispersion of nanoscale second-phase particles are key factors in increasing the strength.
采用简单的热挤压法制备了含Yb的高强镁合金。系统研究了添加Yb对挤压态Mg-4Sm-3Gd(-2Yb)-0.5Zr (SGY0, SGY2)合金动态析出、织构演化、动态再结晶机制、变形机制和强化机制的影响。结果表明:Yb的加入使合金的平均晶粒尺寸由4.17µm减小到1.48µm;这种极端的晶粒细化大大提高了强度。Yb的加入显著促进了相的析出,但没有改变织构类型。非动态再结晶(unrxed)晶粒表现出强烈的基面织构<;011¯1¯0>;与挤出方向平行(ED),而动态再结晶(DRXed)晶粒则呈现较弱的稀土质地,其特征为<;此外,挤压态SGY0和SGY2合金主要发生连续动态再结晶(CDRX),部分DRXed晶粒表现为不连续动态再结晶机制(DDRX)。此外,Yb的加入有利于非基面滑移的激活。挤压态SGY0和SGY2合金中的位错类型包括< a >、< c >和< c + a >位错。然而,SGY2合金具有较高的位错密度,有助于强度的提高。晶粒的极端细化和纳米级第二相颗粒的分散是提高强度的关键因素。
期刊介绍:
The Journal of Magnesium and Alloys serves as a global platform for both theoretical and experimental studies in magnesium science and engineering. It welcomes submissions investigating various scientific and engineering factors impacting the metallurgy, processing, microstructure, properties, and applications of magnesium and alloys. The journal covers all aspects of magnesium and alloy research, including raw materials, alloy casting, extrusion and deformation, corrosion and surface treatment, joining and machining, simulation and modeling, microstructure evolution and mechanical properties, new alloy development, magnesium-based composites, bio-materials and energy materials, applications, and recycling.