Interface microstructure evolution and mechanical properties enhancement of lamellar TC11 alloy under electromagnetic shocking treatment

IF 6.3 2区 材料科学 Q2 CHEMISTRY, PHYSICAL
Qian Sun, Fanglei Wang, Yaxuan Duan, Jue Lu, Lin Hua, Suohui Liang
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Abstract

Interface microstructure plays a key role on the mechanical properties of commercial alloys; however, traditional thermomechanical processing cannot achieve its targeted modification. Herein, a novel electromagnetic shocking treatment (EST) deftly utilizing electromagnetic pulse energy was carried out to selectively tailor the interface microstructure and further enhance the mechanical properties of forged lamellar TC11 alloys. Tensile properties and impact toughness of TC11 alloys were investigated by tensile test and Charpy impact test, respectively. SEM, EBSD, and TEM were used to characterize the phase, grain, and interface complexion variation. The results showed that, with the maximum temperature of alloy sample surface being limited to 354 K, with increasing peak current density, the strength and impact energy of TC11 alloys first increased and then decreased. For EST1 samples with a lower peak current density and sample surface temperature, spheroidization at prior β grain boundaries (GBs) and phase transformation between α and β phases occurred, phase boundary films (PBFs) were frequently observed and α'' phase was detected at PBFs, indicating the occurrence of interface wetting during EST1. It led to the increase in tensile properties and impact energy of alloy samples. Evolution mechanism of spheroidization at prior β GBs and phase transformation between α and β phases were explored in detail. EST-induced interface pre-melting led to the migration, segregation, and redistribution of solute atoms, which promoted phase transformation. It also caused interface migration and then facilitated spheroidization. Next, for EST2 samples with a slightly higher peak current density and sample surface temperature, grains underwent slight coarsening, which mainly contributed to the slight decrease in tensile properties and impact energy of the alloy samples. This study demonstrates that EST can serve as a novel method for targeted regulation of the interface microstructure and further improvement in mechanical properties of TC11 alloys.

Abstract Image

电磁冲击处理下片层TC11合金界面组织演变及力学性能增强
界面组织对工业合金的力学性能起着关键作用;然而,传统的热机械加工无法实现其有针对性的改性。本文采用一种新颖的电磁冲击处理方法,巧妙地利用电磁脉冲能量,有选择地调整界面组织,进一步提高锻造层状TC11合金的力学性能。分别通过拉伸试验和Charpy冲击试验研究了TC11合金的拉伸性能和冲击韧性。利用扫描电子显微镜(SEM)、电子衍射衍射仪(EBSD)和透射电子显微镜(TEM)表征了相、晶粒和界面肤色的变化。结果表明:在合金试样表面最高温度为354k的条件下,随着峰值电流密度的增大,TC11合金的强度和冲击能先升高后降低;对于峰值电流密度较低、表面温度较低的EST1样品,在前期β晶界处发生球化,α相和β相发生相变,频繁观察到相边界膜(PBFs),在PBFs处检测到α”相,表明EST1过程中发生了界面润湿。导致合金试样的拉伸性能和冲击能提高。详细探讨了β - GBs球化的演化机制和α - β相相变过程。est诱导的界面预熔导致溶质原子的迁移、偏析和重分布,促进了相变。它还引起界面迁移,从而促进球化。其次,对于峰值电流密度和样品表面温度稍高的EST2样品,晶粒发生了轻微的粗化,这是合金样品拉伸性能和冲击能略有下降的主要原因。本研究表明,EST可作为一种有针对性地调控TC11合金界面微观组织和进一步改善其力学性能的新方法。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Journal of Alloys and Compounds
Journal of Alloys and Compounds 工程技术-材料科学:综合
CiteScore
11.10
自引率
14.50%
发文量
5146
审稿时长
67 days
期刊介绍: The Journal of Alloys and Compounds is intended to serve as an international medium for the publication of work on solid materials comprising compounds as well as alloys. Its great strength lies in the diversity of discipline which it encompasses, drawing together results from materials science, solid-state chemistry and physics.
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