Yingqing Wang, Chris Grovenor, Susannah Speller, Barbara Shollock, Tayebeh Mousavi
{"title":"X-Ray Computed Tomography Study of the Microstructure of Superconducting MgB2 Bulks","authors":"Yingqing Wang, Chris Grovenor, Susannah Speller, Barbara Shollock, Tayebeh Mousavi","doi":"10.1007/s10948-025-06933-8","DOIUrl":null,"url":null,"abstract":"<div><p>MgB<sub>2</sub> is a promising candidate for commercial superconducting applications because, as grain boundaries in MgB<sub>2</sub> are not weak links, there are fewer limitations on the choice of processing technique compared to high-temperature superconducting (HTS) cuprates. MgB<sub>2</sub> bulks are usually manufactured by powder processing techniques followed by a sintering process. After sintering, the impurity phases such as MgO and MgB<sub>4</sub> along with porosity are formed which strongly affect the superconducting properties mainly the macroscopic path for supercurrent in MgB<sub>2</sub> bulks. Investigation of these microstructural features is essential to improve the superconducting properties of these bulks. In this work, high-resolution laboratory X-ray computed tomography (XCT) has been used to investigate the microstructure of MgB<sub>2</sub> bulks in three dimensions. The volume fraction of defects and impurity phases along with the size distribution of pores have been studied using this advanced technique. A comparison has been made between the data extracted from conventional characterization techniques such as XRD and SEM and those obtained from the advanced XCT analysis.</p></div>","PeriodicalId":669,"journal":{"name":"Journal of Superconductivity and Novel Magnetism","volume":"38 2","pages":""},"PeriodicalIF":1.6000,"publicationDate":"2025-02-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s10948-025-06933-8.pdf","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Superconductivity and Novel Magnetism","FirstCategoryId":"101","ListUrlMain":"https://link.springer.com/article/10.1007/s10948-025-06933-8","RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"PHYSICS, APPLIED","Score":null,"Total":0}
引用次数: 0
Abstract
MgB2 is a promising candidate for commercial superconducting applications because, as grain boundaries in MgB2 are not weak links, there are fewer limitations on the choice of processing technique compared to high-temperature superconducting (HTS) cuprates. MgB2 bulks are usually manufactured by powder processing techniques followed by a sintering process. After sintering, the impurity phases such as MgO and MgB4 along with porosity are formed which strongly affect the superconducting properties mainly the macroscopic path for supercurrent in MgB2 bulks. Investigation of these microstructural features is essential to improve the superconducting properties of these bulks. In this work, high-resolution laboratory X-ray computed tomography (XCT) has been used to investigate the microstructure of MgB2 bulks in three dimensions. The volume fraction of defects and impurity phases along with the size distribution of pores have been studied using this advanced technique. A comparison has been made between the data extracted from conventional characterization techniques such as XRD and SEM and those obtained from the advanced XCT analysis.
期刊介绍:
The Journal of Superconductivity and Novel Magnetism serves as the international forum for the most current research and ideas in these fields. This highly acclaimed journal publishes peer-reviewed original papers, conference proceedings and invited review articles that examine all aspects of the science and technology of superconductivity, including new materials, new mechanisms, basic and technological properties, new phenomena, and small- and large-scale applications. Novel magnetism, which is expanding rapidly, is also featured in the journal. The journal focuses on such areas as spintronics, magnetic semiconductors, properties of magnetic multilayers, magnetoresistive materials and structures, magnetic oxides, etc. Novel superconducting and magnetic materials are complex compounds, and the journal publishes articles related to all aspects their study, such as sample preparation, spectroscopy and transport properties as well as various applications.