{"title":"[Study of the features of perchlozon isolation from biological fluids for the purposes of chemico-toxicological analysis].","authors":"S S Konovalova, E A Illarionova, N V Chmelevskaya","doi":"10.17116/sudmed20246706138","DOIUrl":null,"url":null,"abstract":"<p><strong>The study objective: </strong>Is to develop a methodology for extraction, identification and quantification of perchlozon from biological fluids for the purposes of chemico-toxicological analysis. The article describes the selection of optimal conditions for sample preparation, allowing to extract the perchlozon most effectively. The methodology is tested on model mixtures of biological fluids (urine, saliva, blood plasma). Identification and quantification were performed using UV spectrophotometry and high-performance liquid chromatography.</p>","PeriodicalId":35704,"journal":{"name":"Sudebno-Meditsinskaya Ekspertisa","volume":"67 6","pages":"38-41"},"PeriodicalIF":0.0000,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Sudebno-Meditsinskaya Ekspertisa","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.17116/sudmed20246706138","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"Medicine","Score":null,"Total":0}
引用次数: 0
Abstract
The study objective: Is to develop a methodology for extraction, identification and quantification of perchlozon from biological fluids for the purposes of chemico-toxicological analysis. The article describes the selection of optimal conditions for sample preparation, allowing to extract the perchlozon most effectively. The methodology is tested on model mixtures of biological fluids (urine, saliva, blood plasma). Identification and quantification were performed using UV spectrophotometry and high-performance liquid chromatography.
期刊介绍:
The journal is concerned with the theory and practice of forensic medicine - the problems of thanatology, traumatology, toxicology, serology, forensic obstetrics, forensic dentistry, forensic psychiatry, forensic chemistry, physicotechnical methods of investigation, history of forensic medicine and some problems of criminology and legal laws related to forensic medicine. It publishes original studies by Russian authors, casuistry surveys, abstracts and reviews of Russian and foreign literature, scientific information, reports on scientific conferences.