Exploring the fracture toughness and fatigue crack growth behavior of MoRe alloys

IF 4.2 2区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
Simon Pillmeier , Stanislav Žák , Reinhard Pippan , Jürgen Eckert , Anton Hohenwarter
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Abstract

The fracture and fatigue crack growth behavior of two molybdenum alloys, containing 41 wt-% and 47.5 wt-% rhenium, respectively, are investigated. These alloys were provided in form of cold-wrought rods of 6 mm diameter and exhibit a refined microstructure with highly elongated grains and a strong fiber texture. Similarly processed pure molybdenum was used as reference material and exhibits a significantly coarser microstructure. SEN(T) and C(T) specimens were tested with R-L and L-R orientation. In both, quasi-static and fatigue crack growth experiments, L-R oriented cracks immediately kinked by 90° into the direction of grain elongation. This yields fracture toughness values and effective and long crack threshold values about twice as high as for R-L oriented cracks, which is in good agreement with calculations of a reduced local crack driving force. In both MoRe alloys a cyclic R-curve behavior was captured in fatigue crack growth tests at a load ratio of R = 0.1, while for MoRe47.5 it was still present at R = 0.7. This is attributed mainly to the coarser microstructure. The effective thresholds ∆Kth,eff of both MoRe alloys are remarkably low and deviate from a commonly used estimation, especially for the MoRe47.5 material. It is proposed that plasticity in these materials is facilitated by twinning, leading to the emission of partial dislocations from the crack tip. Although no clear microstructural or fractographic evidence was found, a recalculation of ∆Kth,eff considering partial dislocations indicates a good correlation with experimental values.
探索 MoRe 合金的断裂韧性和疲劳裂纹生长行为
本文研究了两种钼合金(铼含量分别为 41 wt-% 和 47.5 wt-%)的断裂和疲劳裂纹生长行为。这些合金是以直径为 6 毫米的冷锻棒材形式提供的,其微观结构精细,晶粒高度拉长,纤维纹理较强。类似加工的纯钼被用作参考材料,其显微结构明显更粗糙。对 SEN(T) 和 C(T) 试样进行了 R-L 和 L-R 取向测试。在准静态和疲劳裂纹生长实验中,L-R 取向裂纹立即向晶粒伸长方向弯曲 90°。由此产生的断裂韧性值以及有效裂纹和长裂纹阈值大约是 R-L 取向裂纹的两倍,这与降低局部裂纹驱动力的计算结果非常吻合。在两种 MoRe 合金中,疲劳裂纹生长试验都捕捉到了 R = 0.1 负载比下的循环 R 曲线行为,而对于 MoRe47.5 而言,R = 0.7 时仍存在这种行为。这主要归因于较粗的微观结构。两种 MoRe 合金的有效阈值 ∆Kth,eff 都非常低,偏离了常用的估计值,尤其是 MoRe47.5 材料。有人提出,这些材料中的塑性是由孪晶促进的,导致部分位错从裂纹尖端释放出来。虽然没有发现明确的微观结构或断裂学证据,但考虑到部分位错而重新计算的 ∆Kth,eff 表明与实验值有很好的相关性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
CiteScore
7.00
自引率
13.90%
发文量
236
审稿时长
35 days
期刊介绍: The International Journal of Refractory Metals and Hard Materials (IJRMHM) publishes original research articles concerned with all aspects of refractory metals and hard materials. Refractory metals are defined as metals with melting points higher than 1800 °C. These are tungsten, molybdenum, chromium, tantalum, niobium, hafnium, and rhenium, as well as many compounds and alloys based thereupon. Hard materials that are included in the scope of this journal are defined as materials with hardness values higher than 1000 kg/mm2, primarily intended for applications as manufacturing tools or wear resistant components in mechanical systems. Thus they encompass carbides, nitrides and borides of metals, and related compounds. A special focus of this journal is put on the family of hardmetals, which is also known as cemented tungsten carbide, and cermets which are based on titanium carbide and carbonitrides with or without a metal binder. Ceramics and superhard materials including diamond and cubic boron nitride may also be accepted provided the subject material is presented as hard materials as defined above.
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