Analysis of volatile compounds of ginger (Zingiber officinale) during far-infrared combined with hot-air drying by GC-MS and MOS e-nose

IF 2.9 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY
Yongsheng Pei, Changzhi Wang, Lin Fan, Guizhong Tian, Shiyuan Miao, Xiangyi Meng, Zhenfeng Li, Wanxiu Xu
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Abstract

In this study, ginger slices were dehydrated through a combination of far-infrared radiation and hot-air drying (FIR-HAD). The changes in volatile composition were subsequently identified using gas chromatography-mass spectrometry (GC-MS) and metal oxide semiconductor electronic nose (MOS e-nose). The GC-MS analysis revealed that terpenes comprised over 75% of volatile compounds in all examined samples, with zingiberene, β-sesquiphellandrene, and (E, E)-α-farnesene being the dominant constituents. Fresh ginger contained a higher relative proportion compared to dried samples. After FIR-HAD treatment, the terpene levels decreased by 11.9%, 8.9%, 13.7%, and 18.2% at 50 °C, 60 °C, 70 °C, and 80 °C, respectively. Among the various drying conditions, ginger subjected to FIR-HAD at 60 °C displayed the highest concentrations of volatile compounds and exhibited flavor characteristics closest to those of fresh samples. The flavor profiles were further evaluated using MOS e-nose analysis. The terpene compounds demonstrated a strong correlation with the response values of W1W and W2W sensors according to partial least squares regression models. In addition, the concentrations of 6-gingerol, 8-gingerol, and 10-gingerol in ginger exposed to FIR-HAD at 60 °C were also higher compared to other drying conditions. This indicated that the FIR-HAD at 60 °C is more suitable for producing dried ginger with remaining flavor attributes. These findings offer theoretical insights into the changes in volatile compounds of ginger slices during the FIR-HAD procedure. They also highlight the potential for improving drying efficiency through aroma online control techniques in future research.

利用 GC-MS 和 MOS 电子鼻分析生姜(Zingiber officinale)在远红外结合热风干燥过程中的挥发性化合物
在这项研究中,生姜片通过远红外辐射和热风干燥(FIR-HAD)相结合的方法进行脱水。随后使用气相色谱-质谱联用仪(GC-MS)和金属氧化物半导体电子鼻(MOS e-nose)对挥发性成分的变化进行了鉴定。气相色谱-质谱分析表明,在所有检测样品中,萜烯类化合物占挥发性化合物的 75% 以上,其中最主要的成分是辛夷烯、β-鞘氨醇和(E,E)-α-法呢烯。与干燥样品相比,新鲜生姜中的相对比例更高。经过 FIR-HAD 处理后,萜烯含量在 50 ℃、60 ℃、70 ℃ 和 80 ℃ 下分别降低了 11.9%、8.9%、13.7% 和 18.2%。在不同的干燥条件下,60 °C的FIR-HAD条件下生姜的挥发性化合物浓度最高,风味特征最接近新鲜样品。使用 MOS 电子鼻分析法对风味特征进行了进一步评估。根据偏最小二乘法回归模型,萜烯化合物与 W1W 和 W2W 传感器的响应值有很强的相关性。此外,与其他干燥条件相比,在 60 °C的FIR-HAD条件下,生姜中6-姜酚、8-姜酚和10-姜酚的浓度也更高。这表明,60 °C下的FIR-HAD更适于生产具有其余风味特性的干姜。这些发现从理论上揭示了 FIR-HAD 过程中生姜片挥发性化合物的变化。它们还强调了在未来研究中通过香气在线控制技术提高干燥效率的潜力。
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来源期刊
Journal of Food Measurement and Characterization
Journal of Food Measurement and Characterization Agricultural and Biological Sciences-Food Science
CiteScore
6.00
自引率
11.80%
发文量
425
期刊介绍: This interdisciplinary journal publishes new measurement results, characteristic properties, differentiating patterns, measurement methods and procedures for such purposes as food process innovation, product development, quality control, and safety assurance. The journal encompasses all topics related to food property measurement and characterization, including all types of measured properties of food and food materials, features and patterns, measurement principles and techniques, development and evaluation of technologies, novel uses and applications, and industrial implementation of systems and procedures.
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