Influence of the surface energy of a basalt fiber on capillary wicking and in-plane permeability of reinforcements

IF 8.1 2区 材料科学 Q1 ENGINEERING, MANUFACTURING
Romain Ravel , Monica Francesca Pucci , Pierre-Jacques Liotier
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Abstract

This study evaluates the influence of a thermal treatment of a basalt fiber on capillary wicking tests and in-plane permeability experiments, under several pressure differences. The impact of the treatment was characterized at three scales: microscopic, to determine the fiber surface energy; mesoscopic, to estimate an equivalent capillary pressure (Pcap) of the fabric in spontaneous impregnation; and macroscopic, to determine the saturated (Ksat) and unsaturated (Kunsat) permeability of the fibrous preform at the process scale. Results at the microscopic scale showed that the thermal treatment increased the polarity of the fiber by 22% and decreased its surface roughness. Capillary wicking tests showed that the treated fabric presents a better affinity with water, increasing Pcap by 68%. At the process scale, permeability experiments showed the increase of Ksat and Kunsat after treatment. Finally, results of capillary pressure (ΔPγ) showed a dominance of capillary effects under the negative pressure difference.
玄武岩纤维表面能对毛细管吸水和加固材料面内渗透性的影响
本研究评估了玄武岩纤维热处理对毛细管吸水试验和几种压力差下平面渗透性实验的影响。热处理的影响体现在三个方面:微观方面,确定纤维的表面能;中观方面,估算织物在自发浸渍过程中的等效毛细管压力(Pcap);宏观方面,确定纤维预型件在加工过程中的饱和渗透率(Ksat)和非饱和渗透率(Kunsat)。微观结果显示,热处理使纤维的极性增加了 22%,并降低了其表面粗糙度。毛细管吸水测试表明,经过处理的织物与水的亲和性更好,Pcap 增加了 68%。在工艺尺度上,渗透性实验表明,经过处理后,Ksat 和 Kunsat 都有所增加。最后,毛细管压力(ΔPγ)结果表明,在负压差条件下,毛细管效应占主导地位。
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来源期刊
Composites Part A: Applied Science and Manufacturing
Composites Part A: Applied Science and Manufacturing 工程技术-材料科学:复合
CiteScore
15.20
自引率
5.70%
发文量
492
审稿时长
30 days
期刊介绍: Composites Part A: Applied Science and Manufacturing is a comprehensive journal that publishes original research papers, review articles, case studies, short communications, and letters covering various aspects of composite materials science and technology. This includes fibrous and particulate reinforcements in polymeric, metallic, and ceramic matrices, as well as 'natural' composites like wood and biological materials. The journal addresses topics such as properties, design, and manufacture of reinforcing fibers and particles, novel architectures and concepts, multifunctional composites, advancements in fabrication and processing, manufacturing science, process modeling, experimental mechanics, microstructural characterization, interfaces, prediction and measurement of mechanical, physical, and chemical behavior, and performance in service. Additionally, articles on economic and commercial aspects, design, and case studies are welcomed. All submissions undergo rigorous peer review to ensure they contribute significantly and innovatively, maintaining high standards for content and presentation. The editorial team aims to expedite the review process for prompt publication.
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