GGR Handbook of Rock and Mineral Analysis Chapter 7 Quadrupole Inductively Coupled Plasma-Mass Spectrometry

IF 2.7 2区地球科学 Q2 GEOCHEMISTRY & GEOPHYSICS

Geostandards and Geoanalytical Research Pub Date : 2024-10-07 DOI:10.1111/ggr.12556

Kathryn L. Linge

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Abstract

This chapter (Quadrupole Inductively Coupled Plasma-Mass Spectrometry) is a contribution to the Geostandards and Geoanalytical Research Handbook of Rock and Mineral Analysis – an online textbook that is a fully revised and updated edition of Handbook of the Silicate Rock Analysis (P. J. Potts, 1987, Blackie, Glasgow).

Chapter 7 (from Section 2 of the handbook dealing with techniques for the determination of major and trace elements) describes both the history of ICP-MS, including development of the plasma sampling interface and the operation of modern ICP-MS instrumentation. Given their central importance to ICP-MS operation, ion extraction through the sampling interface, ion transmission, ion separation (with a particular focus on the quadrupole mass filter) and counting are given particular attention. Discussion of the analytical characteristics of ICP-MS particularly focusses on spectroscopic interferences (and their mitigation). Finally, an overview of geochemical analysis by ICP-MS considers drift correction, calibration strategies, and laser ablation microsampling.

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GGR 岩石和矿物分析手册》第 7 章四极电感耦合等离子体质谱法

本章（四极电感耦合等离子体质谱法）是对《岩石和矿物分析地质标准和地质分析研究手册》的贡献，该在线教科书是《硅酸盐岩石分析手册》（P. J. Potts，1987 年，Blackie，格拉斯哥）的全面修订和更新版。第 7 章（手册第 2 节，关于主要元素和痕量元素的测定技术）介绍了 ICP-MS 的历史，包括等离子采样界面的开发和现代 ICP-MS 仪器的操作。鉴于其对 ICP-MS 操作的核心重要性，通过采样接口提取离子、离子传输、离子分离（特别关注四极杆质量滤波器）和计数受到了特别关注。对 ICP-MS 分析特性的讨论尤其侧重于光谱干扰（及其缓解）。最后，对使用 ICP-MS 进行地球化学分析的概述考虑了漂移校正、校准策略和激光烧蚀微取样。

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来源期刊

Geostandards and Geoanalytical Research 地学-地球科学综合

CiteScore

7.10

自引率

18.40%

发文量

审稿时长

>12 weeks

期刊介绍： Geostandards & Geoanalytical Research is an international journal dedicated to advancing the science of reference materials, analytical techniques and data quality relevant to the chemical analysis of geological and environmental samples. Papers are accepted for publication following peer review.