Solute-induced transition in Poisson's ratio and strength: A phenomenon in additively manufactured Al-Si-Mg alloys

IF 4.8 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING
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引用次数: 0

Abstract

In this study, cubic coupons of AlSi10Mg alloy were printed using the laser powder bed fusion (LPBF) technique. The effect of heating/reheating cycles on solute trapping and partitioning of alloying elements was investigated using atom probe tomography and transmission electron microscopy. Nano-hardness analysis and uniaxial tensile tests equipped with digital image correlation were employed to investigate the mechanical properties and Poisson's ratio. X-ray micro-computed tomography was utilized to detect strain localization sites along the building direction. Also, the uniaxial tensile test was simulated using finite element analysis to verify the experimental data and predict stress triaxiality. The results showed that the solute trapping and partitioning during the LPBF process results in remarkable changes in phases, their size and morphology, Poisson's ratio, strengthening factor, and consequently mechanical properties. While the tensile sample from top part of the LPBF coupon mostly shows porosity due to floating and entrapment of gases during layer-by-layer fusion/solidification, the sample from bottom part is exposed to sub-surface microcracking induced by residual stresses. The hardness, elastic, and shear moduli, Peierls stress, and cumulative strain energy of the top-part sample are higher than those of the bottom-part sample even though electron backscatter diffraction analyses report similar grain size and texture. Besides, by distancing from the build plate, the Poisson's ratio decreases. Simulation results of both samples indicate that the middle of the gauge is a high-potential area of failure initiation, where the bottom-part sample shows higher stress localization.
溶质诱导的泊松比和强度转变:添加式制造的铝硅镁合金中的一种现象
在这项研究中,使用激光粉末床熔融(LPBF)技术打印了 AlSi10Mg 合金立方体试样。利用原子探针断层扫描和透射电子显微镜研究了加热/再加热循环对溶质捕获和合金元素分配的影响。采用纳米硬度分析和配备数字图像相关技术的单轴拉伸试验来研究机械性能和泊松比。利用 X 射线微型计算机断层扫描来检测沿建筑方向的应变定位点。此外,还利用有限元分析模拟了单轴拉伸试验,以验证实验数据并预测应力三轴性。结果表明,在 LPBF 过程中,溶质截留和分配导致相、相的大小和形态、泊松比、强化因子以及机械性能发生显著变化。LPBF 试样上部的拉伸试样大多因逐层熔融/凝固过程中气体的漂浮和夹带而出现孔隙,而下部的试样则因残余应力而出现表层下的微裂纹。尽管电子反向散射衍射分析显示出相似的晶粒尺寸和纹理,但上部样品的硬度、弹性和剪切模量、Peierls 应力以及累积应变能均高于下部样品。此外,与构建板的距离越远,泊松比越小。两种样品的模拟结果表明,量规的中部是失效的高发区,而底部样品的应力定位更高。
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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