Experimental investigation and micromechanical analysis of glass fiber reinforced polyamide 6

IF 3.4 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
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Abstract

Achieving process stability in the thermoforming of fiber reinforced polymer materials (FRPs) for aerospace or automotive manufacturing is usually associated with a costly trial-and-error process, where experimental boundary conditions and other influencing factors, such as, for example, material composition, need to be adjusted over time. This is especially true when material phenomena on the microlevel, such as the crystallization kinetics of the polymer matrix or resulting stresses from temperature gradients, are the cause of the process instability. To reduce the experimental effort and reliably predict the material behavior during thermoforming, finite element simulation tools on multiple scales are a useful solution. Hereby, incorporating micromechanical phenomena into the model approaches is crucial for an accurate prediction by further reducing the deviation between simulation and experiment, in particular with regard to the underlying nonlinear material behavior. In this work, unit cell simulations on the microscale of a unidirectional glass fiber reinforced polymer (UD GFRP) are conducted to predict effective thermomechanical properties of a single material ply and ascertain the effect of individual ply constituents on the homogenized material behavior. The polymeric matrix material model used was identified in a prior publication with experimental data at various temperatures for polyamide 6 blends with varying degrees of crystallinities. Various randomization methods are tested to generate the unit cells and replicate the composites’ random fiber distribution, with a focus on process automation. The simulative results are successfully compared to an experimental study on glass fiber reinforced polyamide 6 tested at various temperatures, demonstrating the potential of the approach to reduce both time and cost required for material characterization. Finally, the unit cells are used to generate a database to predict untested load cases that will be used in future work to characterize a homogenized macroscopic material model.

玻璃纤维增强聚酰胺 6 的实验研究和微机械分析
在用于航空航天或汽车制造的纤维增强聚合物材料(FRP)热成型过程中,要实现工艺稳定性通常需要进行成本高昂的反复试验,其中实验边界条件和其他影响因素(如材料成分)需要随着时间的推移而不断调整。当微观层面的材料现象(如聚合物基体的结晶动力学或温度梯度产生的应力)是造成工艺不稳定的原因时,情况更是如此。为了减少实验工作量并可靠地预测热成型过程中的材料行为,多尺度有限元模拟工具是一种有用的解决方案。因此,将微观机械现象纳入模型方法对于准确预测至关重要,可进一步减少模拟与实验之间的偏差,特别是在潜在的非线性材料行为方面。在这项工作中,对单向玻璃纤维增强聚合物(UD GFRP)进行了微尺度单元格模拟,以预测单个材料层的有效热机械性能,并确定单个层成分对均质材料行为的影响。所使用的聚合物基体材料模型是在之前的出版物中通过不同结晶度的聚酰胺 6 混合物在不同温度下的实验数据确定的。测试了各种随机化方法,以生成单元格并复制复合材料的随机纤维分布,重点关注过程自动化。模拟结果成功地与在不同温度下测试的玻璃纤维增强聚酰胺 6 的实验研究进行了比较,证明了该方法在减少材料表征所需的时间和成本方面的潜力。最后,单元格被用于生成一个数据库,以预测未经测试的载荷情况,这些载荷情况将在未来的工作中用于表征均质宏观材料模型。
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来源期刊
Mechanics of Materials
Mechanics of Materials 工程技术-材料科学:综合
CiteScore
7.60
自引率
5.10%
发文量
243
审稿时长
46 days
期刊介绍: Mechanics of Materials is a forum for original scientific research on the flow, fracture, and general constitutive behavior of geophysical, geotechnical and technological materials, with balanced coverage of advanced technological and natural materials, with balanced coverage of theoretical, experimental, and field investigations. Of special concern are macroscopic predictions based on microscopic models, identification of microscopic structures from limited overall macroscopic data, experimental and field results that lead to fundamental understanding of the behavior of materials, and coordinated experimental and analytical investigations that culminate in theories with predictive quality.
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