Stepwise Multi-Temperature Thermogravimetric Analysis (SMT-TGA) for Rapid Alloy Development

IF 2.1 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING
Daniel Monceau, Hugo Enjalbert, Clara Desgranges, Tom Sanviemvongsak, Antoine Casadebaigt, Thomas Perez
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引用次数: 0

Abstract

A stepwise multi-temperature thermogravimetric analysis (SMT-TGA) method is a rapid and time- and material-efficient measurement procedure for oxidation kinetics over a wide range of temperatures. It is suitable for alloy design and material selection procedures. It involves subjecting a sample to a series of steps at increasing temperatures, followed by steps at decreasing temperatures to identify possible effects on the evolution of oxide layer microstructures on oxidation kinetics. This method has been tested for a wide range of metallic alloys in the present work, allowing for the mapping of possible ranges of parabolic oxidation kinetics of industrial alloys between 600 and 1300°C. Two examples of effects of thermal history have also been described in this publication.

Abstract Image

用于快速合金开发的逐步式多温热重分析 (SMT-TGA)
分步多温热重分析法(SMT-TGA)是一种快速、省时、省材料的测量方法,可用于测量宽温度范围内的氧化动力学。它适用于合金设计和材料选择程序。该方法是将样品置于一系列温度升高的步骤中,然后再置于温度降低的步骤中,以确定氧化层微结构的演变对氧化动力学可能产生的影响。在目前的工作中,已对多种金属合金进行了测试,从而绘制出 600 至 1300°C 之间工业合金抛物线氧化动力学的可能范围。本出版物还介绍了热历史影响的两个实例。
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来源期刊
Oxidation of Metals
Oxidation of Metals 工程技术-冶金工程
CiteScore
5.10
自引率
9.10%
发文量
47
审稿时长
2.2 months
期刊介绍: Oxidation of Metals is the premier source for the rapid dissemination of current research on all aspects of the science of gas-solid reactions at temperatures greater than about 400˚C, with primary focus on the high-temperature corrosion of bulk and coated systems. This authoritative bi-monthly publishes original scientific papers on kinetics, mechanisms, studies of scales from structural and morphological viewpoints, transport properties in scales, phase-boundary reactions, and much more. Articles may discuss both theoretical and experimental work related to gas-solid reactions at the surface or near-surface of a material exposed to elevated temperatures, including reactions with oxygen, nitrogen, sulfur, carbon and halogens. In addition, Oxidation of Metals publishes the results of frontier research concerned with deposit-induced attack. Review papers and short technical notes are encouraged.
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