Enhancing Creep Resistance of Powder-Metallurgy Near-β Titanium Alloy via Rapid Heat Treatment Followed by Aging

IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
Fucheng Qiu, Tuo Cheng, Dmytro G. Savvakin, Orest M. Ivasishin
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Abstract

In this work, rapid heat treatment followed by aging (RHTA) was proposed to improve the creep properties of Ti-5Al-5Mo-5 V-1Cr-1Fe alloy produced by sintering and hot deformation of blended elemental powder compacts. At 400 °C., the stress exponents of alloy after annealing and RHTA are 2.66 and 3.05. At the stress of 300 MPa with temperatures in the range of 400-500 °C., the activation energies of alloy after annealing and RHTA are 192.1 kJ/mol and 223.0 kJ/mol, respectively. The stress exponents and activation energies indicate that the creep in specimens after annealing and RHTA was mainly affected by dislocation climb, which has been proved by the jogged screw dislocations observed by TEM. The fine α lamellae obtained by RHTA contributed to the evidently better creep resistance than that of the alloy with equiaxed structure after hot rolling and annealing. Importantly, the results confirmed that the bimodal microstructure obtained by RHTA can achieve better creep resistance than full lamellae structure obtained by traditional heat treatment.

Abstract Image

通过快速热处理和时效处理提高粉末冶金近 β 钛合金的抗蠕变性
本研究提出了先快速热处理后时效(RHTA)的方法,以改善通过混合元素粉末压块烧结和热变形生产的 Ti-5Al-5Mo-5 V-1Cr-1Fe 合金的蠕变性能。400 °C 时,退火和 RHTA 后合金的应力指数分别为 2.66 和 3.05。在应力为 300 兆帕,温度为 400-500 ℃的条件下,合金退火后的活化能和 RHTA 的活化能分别为 192.1 kJ/mol 和 223.0 kJ/mol。应力指数和活化能表明,退火和 RHTA 后试样的蠕变主要受位错攀升的影响,这一点已被 TEM 观察到的点状螺位错所证实。与热轧和退火后的等轴晶结构合金相比,RHTA 得到的细α层状结构使合金的抗蠕变性能明显更好。重要的是,研究结果证实,通过 RHTA 获得的双峰微观结构比通过传统热处理获得的全层状结构具有更好的抗蠕变性。
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来源期刊
Journal of Materials Engineering and Performance
Journal of Materials Engineering and Performance 工程技术-材料科学:综合
CiteScore
3.90
自引率
13.00%
发文量
1120
审稿时长
4.9 months
期刊介绍: ASM International''s Journal of Materials Engineering and Performance focuses on solving day-to-day engineering challenges, particularly those involving components for larger systems. The journal presents a clear understanding of relationships between materials selection, processing, applications and performance. The Journal of Materials Engineering covers all aspects of materials selection, design, processing, characterization and evaluation, including how to improve materials properties through processes and process control of casting, forming, heat treating, surface modification and coating, and fabrication. Testing and characterization (including mechanical and physical tests, NDE, metallography, failure analysis, corrosion resistance, chemical analysis, surface characterization, and microanalysis of surfaces, features and fractures), and industrial performance measurement are also covered
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