Shape Anisotropy of Grains Formed by Laser Melting of (CoCuFeZr)17Sm2

Abstract

For permanent magnetic materials, anisotropic microstructures are crucial for maximizing remanence Jr and maximum energy product (BH)max. This also applies to additive manufacturing processes such as laser powder bed fusion (PBF-LB). In PBF-LB processing, the solidification behavior is determined by the crystal structure of the material, the substrate, and the melt-pool morphology, resulting from the laser power PL and scanning speed vs. To study the impact of these parameters on the textured growth of grains in the melt-pool, experiments were conducted using single laser tracks on (CoCuFeZr)17Sm2 sintered magnets. A method was developed to quantify this grain shape anisotropy from electron backscatter diffraction (EBSD) analysis. For all grains in the melt-pool, the grain shape aspect ratio (GSAR) is calculated to distinguish columnar (GSAR < 0.5) and equiaxed (GSAR > 0.5) grains. For columnar grains, the grain shape orientation (GSO) is determined. The GSO represents the preferred growth direction of each grain. This method can also be used to reconstruct the temperature gradients present during solidification in the melt-pool. A dependence of the melt-pool aspect ratio (depth/width) on energy input was observed, where increasing energy input (increasing PL, decreasing vs) led to higher aspect ratios. For aspect ratios around 0.3, an optimum for directional columnar growth (93% area fraction) with predominantly vertical growth direction (mean angular deviation of 23.1° from vertical) was observed. The resulting crystallographic orientation is beyond the scope of this publication and will be investigated in future work.