Influence of Crystal Orientation on Freckle Formation in Single Crystal Heavy-Plate Castings

Weiguo Jiang, Dongyu Han, Lin Dong, Kaiwen Li, Xiangbin Meng, Qiang Li
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Abstract

The effect of the crystal orientation on freckle formation has been investigated in single crystal Ni-base superalloy heavy-plate castings. Single crystal superalloy heavy-plate castings grown along the <001> , <011> and <111> crystallographic orientations were prepared by the bottom seeding technique and Bridgman method. Optical microscopy (OM) and scanning electron microscopy (SEM) were employed to observe the microstructure, and electron backscatter diffraction (EBSD) was used to characterize the crystallographic orientation of the castings. The morphology of the mushy zone during directional solidification was simulated by ProCAST finite element software. The experimental results show that the space between primary dendrites at the (010) crystal plane of <011> oriented plate casting and the (100) crystal plane of <111> oriented plate casting is wider than that at the same corresponding crystal plane of <001> oriented plate casting. The occurrence of freckles depends not only on orientation but also on dendrite morphology. Compared with orientation, the freckle is more sensitive to dendrite morphology and the space between primary dendrites of the single crystal plates. The freckle formation tendency of the <001> orientation casting was the weakest among the three crystal orientation castings, and the reason for this tendency was discussed.

Graphical Abstract

Abstract Image

晶体取向对单晶重板铸件中雀斑形成的影响
研究了单晶镍基超级合金重型铸件中晶体取向对雀斑形成的影响。采用底部播种技术和布里奇曼法制备了沿<001>、<011>和<111>晶向生长的单晶超合金重型铸件。采用光学显微镜(OM)和扫描电子显微镜(SEM)观察微观结构,并利用电子反向散射衍射(EBSD)表征铸件的结晶取向。利用 ProCAST 有限元软件模拟了定向凝固过程中粘稠区的形态。实验结果表明,取向平板铸件 (010) 晶面和取向平板铸件 (111>) (100) 晶面的原生枝晶之间的空间比取向平板铸件 (<001>) 相同晶面的原生枝晶之间的空间要宽。雀斑的出现不仅取决于取向,还取决于枝晶形态。与取向相比,雀斑对单晶板的枝晶形态和主枝晶之间的空间更为敏感。在三种晶体取向铸件中,<001>取向铸件的雀斑形成趋势最弱,并讨论了这种趋势的原因。
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