Influence of Oxidation Temperature on the Tensile Behaviour in a 2.5 D Needled Carbon/Carbon Composite for Aircraft Brakes

IF 2.1 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING
Théo Zubiaurre, Matteo Lunghi, Jérome Favergeon, Zoheir Aboura
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Abstract

An air-oxidized carbon/carbon (c/c) composite was studied under tensile conditions to examine oxidation temperature’s influence on its behaviour and on the residual mechanical properties. Three oxidation temperatures were tested with oxidation duration chosen to obtain the same weight loss on the samples at each temperature. Notable differences were found in the material’s behaviour depending on the oxidation temperatures. These results show that the weight loss criterion commonly used in the literature to quantify c/c composite oxidation needs to be complete to reflect the actual state of the material after oxidation. Microscopic observations revealed different oxidation patterns that underlined a heterogeneous consumption of the material from one temperature to another. Consequently, a non-destructive-test based on ultrasonic signals was explored in order to complete the weight loss criterion. Variations of weight loss at each exposure oxidation temperature were correctly assessed, and the technique was able to discriminate the oxidation temperatures above 5% of weight loss. The low-temperature oxidation behaviour is discussed and an explanation based on a variation on the attack of the fibre/matrix interfaces that could explain the difference of the tensile behaviour is proposed.

Abstract Image

Abstract Image

氧化温度对飞机制动器用 2.5 D 针状碳/碳复合材料拉伸行为的影响
在拉伸条件下对空气氧化碳/碳(c/c)复合材料进行了研究,以考察氧化温度对其行为和残余机械性能的影响。测试了三种氧化温度,氧化持续时间的选择是为了在每个温度下获得相同的样品重量损失。根据氧化温度的不同,材料的性能也有显著差异。这些结果表明,文献中常用来量化 c/c 复合材料氧化的失重标准必须完全反映材料氧化后的实际状态。显微镜观察显示了不同的氧化模式,凸显了材料在不同温度下的异质消耗。因此,我们探索了一种基于超声波信号的非破坏性测试方法,以完善失重标准。正确评估了每个暴露氧化温度下的重量损失变化,该技术能够区分重量损失超过 5%的氧化温度。对低温氧化行为进行了讨论,并提出了一种基于纤维/基质界面侵蚀变化的解释,可以解释拉伸行为的差异。
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来源期刊
Oxidation of Metals
Oxidation of Metals 工程技术-冶金工程
CiteScore
5.10
自引率
9.10%
发文量
47
审稿时长
2.2 months
期刊介绍: Oxidation of Metals is the premier source for the rapid dissemination of current research on all aspects of the science of gas-solid reactions at temperatures greater than about 400˚C, with primary focus on the high-temperature corrosion of bulk and coated systems. This authoritative bi-monthly publishes original scientific papers on kinetics, mechanisms, studies of scales from structural and morphological viewpoints, transport properties in scales, phase-boundary reactions, and much more. Articles may discuss both theoretical and experimental work related to gas-solid reactions at the surface or near-surface of a material exposed to elevated temperatures, including reactions with oxygen, nitrogen, sulfur, carbon and halogens. In addition, Oxidation of Metals publishes the results of frontier research concerned with deposit-induced attack. Review papers and short technical notes are encouraged.
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