Development of a versatile method for predicting the density of monocomponent dry fine materials compacts based on comparative study of compression factors

IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL
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Abstract

This paper represents the study of the influence of technological factors and particles properties on the compression of dry powders. Using two-factor analysis of variance (ANOVA) method, the influence of powder material and particle sizes on the compression intensity factor was compared. Relations between the compressibility of powders and thermodynamic, thermal (melting point, heat of sublimation, etc.), mechanical (Young's modulus, shear modulus, hardness, etc.) and energy characteristics of the substance of the particles (energy of the crystal ion lattice, energy of atomization, energy of the core-electron interaction) have been obtained. Based on the these dependencies, a multiple regression model of the combined effect of the energy and structural characteristics of the particles' crystal lattice on the compressibility of a powder was constructed. Using the obtained dependencies, a versatile method for predicting the density of dry powder compacts depending on the applied pressing pressure was developed.

Abstract Image

基于压缩系数比较研究,开发预测单组分干细材料压实密度的通用方法
本文研究了技术因素和颗粒特性对干粉压缩的影响。采用双因素方差分析(ANOVA)方法,比较了粉末材料和颗粒大小对压缩强度系数的影响。得出了粉末的可压缩性与热力学、热学(熔点、升华热等)、机械学(杨氏模量、剪切模量、硬度等)和颗粒物质的能量特性(晶体离子晶格的能量、雾化能量、核-电子相互作用的能量)之间的关系。基于这些依赖关系,我们构建了颗粒晶格的能量和结构特征对粉末可压缩性的综合影响的多元回归模型。利用所获得的依赖关系,开发出了一种预测干粉压实密度的通用方法,该方法取决于所施加的加压压力。
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来源期刊
Powder Technology
Powder Technology 工程技术-工程:化工
CiteScore
9.90
自引率
15.40%
发文量
1047
审稿时长
46 days
期刊介绍: Powder Technology is an International Journal on the Science and Technology of Wet and Dry Particulate Systems. Powder Technology publishes papers on all aspects of the formation of particles and their characterisation and on the study of systems containing particulate solids. No limitation is imposed on the size of the particles, which may range from nanometre scale, as in pigments or aerosols, to that of mined or quarried materials. The following list of topics is not intended to be comprehensive, but rather to indicate typical subjects which fall within the scope of the journal's interests: Formation and synthesis of particles by precipitation and other methods. Modification of particles by agglomeration, coating, comminution and attrition. Characterisation of the size, shape, surface area, pore structure and strength of particles and agglomerates (including the origins and effects of inter particle forces). Packing, failure, flow and permeability of assemblies of particles. Particle-particle interactions and suspension rheology. Handling and processing operations such as slurry flow, fluidization, pneumatic conveying. Interactions between particles and their environment, including delivery of particulate products to the body. Applications of particle technology in production of pharmaceuticals, chemicals, foods, pigments, structural, and functional materials and in environmental and energy related matters. For materials-oriented contributions we are looking for articles revealing the effect of particle/powder characteristics (size, morphology and composition, in that order) on material performance or functionality and, ideally, comparison to any industrial standard.
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