Marc Ninou Codina , Gernot M. Wallner , Robert Pugstaller , Gabriel Riedl , Bernhard Strauß , Martin Rosner
{"title":"Improvement of the environmental fatigue resistance of epoxy-based electrical steel laminates by pre-treatment of the substrate","authors":"Marc Ninou Codina , Gernot M. Wallner , Robert Pugstaller , Gabriel Riedl , Bernhard Strauß , Martin Rosner","doi":"10.1016/j.ijadhadh.2024.103788","DOIUrl":null,"url":null,"abstract":"<div><p>Electrical generators or engines are based on full surface bonded steel plies. Temperature control is of high relevance to achieve reduced heat dissipations along with improved efficiency. This paper evaluated the effect of service relevant operating conditions (i.e., cooling agents, elevated service temperature and fatigue stresses) on the delamination behavior of electrical steel laminates on specimen and lab level. Therefore, a linear elastic fracture mechanics method and a set-up suitable for superimposed environmental and cyclic fatigue testing was implemented and employed. Two electrical steel laminate configurations were investigated. Pre-treated and un-treated sheets were double side coated with an epoxy varnish. Further, a catalyst was applied on both sides of the coated sheets made from the pre-treated substrate. Double cantilever beam specimens were manufactured by stacking and laminating 6 coated substrates. The fractured surfaces of the fatigue tested specimen were characterized by laser confocal microscopy and infrared spectroscopy in hemispheric reflectance mode. Threshold strain energy release rate values (G<sub>th</sub>) ranging from 16 to 62 J/m<sup>2</sup> were obtained depending on the investigated coated substrates and the environmental conditions. Laminates produced with pre-treated sheets and catalyst exhibited notably enhanced G<sub>th</sub> and decreased rates of crack propagation within the stable crack growth regime. A similar crack growth behavior was ascertained in hot air or oil-based cooling agent. The crossover point of the temperature dependent G<sub>th</sub> values was indicative for the glass transition temperature of the adhesives. The fractured surfaces presented mainly cohesive failure at higher strain energy release rate values followed by mixed cohesive and interfacial failure when approaching to the threshold regime.</p></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"134 ","pages":"Article 103788"},"PeriodicalIF":3.2000,"publicationDate":"2024-07-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S0143749624001702/pdfft?md5=47d019226a4dd9ad99d41f0f4c9edf3a&pid=1-s2.0-S0143749624001702-main.pdf","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Adhesion and Adhesives","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0143749624001702","RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"ENGINEERING, CHEMICAL","Score":null,"Total":0}
引用次数: 0
Abstract
Electrical generators or engines are based on full surface bonded steel plies. Temperature control is of high relevance to achieve reduced heat dissipations along with improved efficiency. This paper evaluated the effect of service relevant operating conditions (i.e., cooling agents, elevated service temperature and fatigue stresses) on the delamination behavior of electrical steel laminates on specimen and lab level. Therefore, a linear elastic fracture mechanics method and a set-up suitable for superimposed environmental and cyclic fatigue testing was implemented and employed. Two electrical steel laminate configurations were investigated. Pre-treated and un-treated sheets were double side coated with an epoxy varnish. Further, a catalyst was applied on both sides of the coated sheets made from the pre-treated substrate. Double cantilever beam specimens were manufactured by stacking and laminating 6 coated substrates. The fractured surfaces of the fatigue tested specimen were characterized by laser confocal microscopy and infrared spectroscopy in hemispheric reflectance mode. Threshold strain energy release rate values (Gth) ranging from 16 to 62 J/m2 were obtained depending on the investigated coated substrates and the environmental conditions. Laminates produced with pre-treated sheets and catalyst exhibited notably enhanced Gth and decreased rates of crack propagation within the stable crack growth regime. A similar crack growth behavior was ascertained in hot air or oil-based cooling agent. The crossover point of the temperature dependent Gth values was indicative for the glass transition temperature of the adhesives. The fractured surfaces presented mainly cohesive failure at higher strain energy release rate values followed by mixed cohesive and interfacial failure when approaching to the threshold regime.
期刊介绍:
The International Journal of Adhesion and Adhesives draws together the many aspects of the science and technology of adhesive materials, from fundamental research and development work to industrial applications. Subject areas covered include: interfacial interactions, surface chemistry, methods of testing, accumulation of test data on physical and mechanical properties, environmental effects, new adhesive materials, sealants, design of bonded joints, and manufacturing technology.