Electrospray crystallization: A review on submicrometric and nanosized crystal synthesis

IF 4.5 2区材料科学 Q1 CRYSTALLOGRAPHY

Progress in Crystal Growth and Characterization of Materials Pub Date : 2024-07-13 DOI:10.1016/j.pcrysgrow.2024.100636

Angelo Oliveira Silva, Alessandro Rogério Paulazzi, Karina Luzia Andrade, Ricardo Antonio Francisco Machado, Cintia Marangoni, Dachamir Hotza

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Abstract

This review presents a comprehensive discussion of the electrospray crystallization process, which represents a combination of electrospraying and crystallization through solvent evaporation, offering an efficient and cost-effective approach for the synthesis of submicrometric and nanosized crystals. Electrospray crystallization has demonstrated a multitude of advantages, including the generation of smaller crystals, enhanced dispersion, and the creation of diverse product morphologies, such as planar and cubic tetragonal structures. These benefits surpass those of conventional electrospraying methods and traditional crystallization mechanisms. This review also provides a historical context of works and highlights the wide array of potential applications. It explores the mechanisms and fundamental concepts related to both electrospraying and crystallization processes. Moreover, it presents an experimental process development proposal, with the aim of charting a course for future applications of advanced crystals, including drug delivery, catalysis, and energy storage.

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电喷雾结晶：亚微米级和纳米级晶体合成综述

本综述全面论述了电喷雾结晶工艺，它是电喷雾和通过溶剂蒸发结晶的结合，为合成亚微米级和纳米级晶体提供了一种高效、经济的方法。电喷雾结晶法具有多种优势，包括生成更小的晶体、增强分散性，以及生成平面和立方四边形结构等多种产品形态。这些优势超越了传统电喷雾方法和传统结晶机制。本综述还介绍了相关工作的历史背景，并强调了广泛的潜在应用。它探讨了与电喷雾和结晶过程相关的机制和基本概念。此外，它还提出了一项实验过程开发建议，旨在为先进晶体的未来应用（包括药物输送、催化和能量存储）指明方向。

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来源期刊

Progress in Crystal Growth and Characterization of Materials 工程技术-材料科学：表征与测试

CiteScore

8.80

自引率

2.00%

发文量

审稿时长

1 day

期刊介绍： Materials especially crystalline materials provide the foundation of our modern technologically driven world. The domination of materials is achieved through detailed scientific research. Advances in the techniques of growing and assessing ever more perfect crystals of a wide range of materials lie at the roots of much of today''s advanced technology. The evolution and development of crystalline materials involves research by dedicated scientists in academia as well as industry involving a broad field of disciplines including biology, chemistry, physics, material sciences and engineering. Crucially important applications in information technology, photonics, energy storage and harvesting, environmental protection, medicine and food production require a deep understanding of and control of crystal growth. This can involve suitable growth methods and material characterization from the bulk down to the nano-scale.