A Comprehensive Study of Method Optimisation of Re-Refining Spent Lubricating Oil

IF 1.8 4区 工程技术 Q3 ENGINEERING, CHEMICAL
Sayantan Sarkar, Deepshikha Datta, Gokulan Ravindiran, Bimal Das
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Abstract

Used lubricating oil is generated by various machinery after extended operation. It is also referred to as spent mobile oil. Extremely hazardous waste lubricating oil is detrimental to the environment because it produces oxidative products when additives break down. Used lubricating oil is classified as a hazardous waste substance and has a negative impact on the environment. Polychlorinated biphenyls (PCBs), carcinogenic substances and other impurities make lubricating oil poisonous and pose a serious threat to human health and the environment. Re-refining is considered the preferred technology for resource conservation, waste minimisation and reduced environmental hazards. The present study focuses on optimising the method of re-refining waste lubricating oil. The effects of various operating parameters such as refining time, refining temperature, solvent-to-used oil ratio and flocculant dosage have been extensively studied to maximise the percentage recovery of lubricating oil. Optimum process parameters are (i) a refining time of 80 min, (ii) a refining temperature of 48°C, (iii) solvent-to-waste oil ratio of 5:1 (w/w) and (iv) a flocculant dosage of 2 g/kg of solvent; the optimum yield was found to be 75% with the solvent extraction method and 78% with the extraction–flocculation method, respectively. The purity and physico-chemical properties of the recovered oil were thoroughly analysed using Fourier transform infrared spectroscopy and ASTM standard methods. It was concluded that refined oil can effectively reduce the ongoing oil crisis and create a clean, healthy environment.

废润滑油再提炼方法优化综合研究
废润滑油是各种机械在长时间运行后产生的。它也被称为废机油。极度危险的废润滑油对环境有害,因为添加剂分解后会产生氧化产物。废润滑油被归类为危险废物,对环境有负面影响。多氯联苯 (PCB)、致癌物质和其他杂质使润滑油有毒,对人类健康和环境构成严重威胁。再精炼被认为是节约资源、减少废物和降低环境危害的首选技术。本研究的重点是优化废弃润滑油的再精炼方法。我们广泛研究了各种操作参数的影响,如精炼时间、精炼温度、溶剂与废油比率和絮凝剂用量,以最大限度地提高润滑油的回收率。最佳工艺参数为:(i) 精炼时间为 80 分钟;(ii) 精炼温度为 48°C;(iii) 溶剂与废油比为 5:1(重量比);(iv) 絮凝剂用量为 2 克/千克溶剂;发现溶剂萃取法的最佳产量为 75%,萃取-絮凝法的最佳产量为 78%。采用傅里叶变换红外光谱法和美国材料试验协会标准方法对回收油的纯度和物理化学性质进行了全面分析。结论是,精炼油可以有效减少当前的石油危机,并创造一个清洁、健康的环境。
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来源期刊
Lubrication Science
Lubrication Science ENGINEERING, CHEMICAL-ENGINEERING, MECHANICAL
CiteScore
3.60
自引率
10.50%
发文量
61
审稿时长
6.8 months
期刊介绍: Lubrication Science is devoted to high-quality research which notably advances fundamental and applied aspects of the science and technology related to lubrication. It publishes research articles, short communications and reviews which demonstrate novelty and cutting edge science in the field, aiming to become a key specialised venue for communicating advances in lubrication research and development. Lubrication is a diverse discipline ranging from lubrication concepts in industrial and automotive engineering, solid-state and gas lubrication, micro & nanolubrication phenomena, to lubrication in biological systems. To investigate these areas the scope of the journal encourages fundamental and application-based studies on: Synthesis, chemistry and the broader development of high-performing and environmentally adapted lubricants and additives. State of the art analytical tools and characterisation of lubricants, lubricated surfaces and interfaces. Solid lubricants, self-lubricating coatings and composites, lubricating nanoparticles. Gas lubrication. Extreme-conditions lubrication. Green-lubrication technology and lubricants. Tribochemistry and tribocorrosion of environment- and lubricant-interface interactions. Modelling of lubrication mechanisms and interface phenomena on different scales: from atomic and molecular to mezzo and structural. Modelling hydrodynamic and thin film lubrication. All lubrication related aspects of nanotribology. Surface-lubricant interface interactions and phenomena: wetting, adhesion and adsorption. Bio-lubrication, bio-lubricants and lubricated biological systems. Other novel and cutting-edge aspects of lubrication in all lubrication regimes.
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