Unusual twin induced recrystallization and corresponding texture optimization in a cold rolled Mg-Gd-Zr alloy during annealing

IF 15.8 1区 材料科学 Q1 METALLURGY & METALLURGICAL ENGINEERING
Ning Lv , Lingyu Zhao , Hong Yan , Boyu Liu , Rongshi Chen , Zhiwei Shan
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Abstract

Twins play an important role in the texture transition during annealing. In a cold rolled high rare earth content magnesium (Mg) alloys with {10–12} extension twins, {11–21} extension twins, {10–11} compression twins and {10–11}-{10–12} double twins and frequent twin-twin interactions, quasi-in-situ electron backscatter diffraction method was used to observe the twin induced static recrystallization (SRX) and related effect on texture during annealing. The results show that basal component was consumed owing to the SRX occurred in basal oriented {10–12} twins and SRXed grains with several specific orientations show preferential grain growth. SRX widely operated in the {10–12} extension and {11–21} extension twins, but absent in most {10–11} compression and {10–11}-{10–12} double twins, which is different to traditional twin induced SRX. Most compression/double twins detwinned while only partial tension twins detwinned. Operation of {11–21} twins and resultant twin-twin interaction facilitate the formation of serrated twin boundaries, which can serve as nucleation sites. Activation of <c + a> dislocation and related dislocation interaction in high dislocation density areas promote the formation of new grain boundaries and related SRX. Profuse <c + a> dislocations in basal oriented twins release the strain accumulation in compression/double twins and thus result in the absence of SRX. The twin size difference, storage energy and dislocation-twin interaction commonly functioned to the detwinning during annealing. The near-coincide site lattice boundaries that show high mobility were considered to be the important contributor to the preferential grain growth of SRXed grains.
冷轧 Mg-Gd-Zr 合金退火过程中的异常孪晶诱导再结晶及相应的组织优化
孪晶在退火过程中的织构转变中起着重要作用。采用准原位电子后向散射衍射方法,对具有{10-12}扩展孪晶、{11-21}扩展孪晶、{10-11}压缩孪晶和{10-11}-{10-12}双孪晶和频繁的孪晶相互作用的冷轧高稀土含量镁(Mg)合金进行了退火过程中孪晶诱导的静态再结晶(SRX)及其对织构的影响。结果表明:{10-12}基向孪晶中SRX的发生消耗了基向组分,具有几种特定取向的SRX晶粒优先生长。SRX在{10-12}伸展孪晶和{11-21}伸展孪晶中广泛存在,而在大多数{10-11}压缩孪晶和{10-11}-{10-12}双孪晶中不存在,这与传统孪晶诱导的SRX不同。大多数压缩孪晶是双孪晶,而只有部分张力孪晶是双孪晶。{11-21}孪晶的作用和由此产生的孪晶相互作用促进了锯齿孪晶晶界的形成,这些晶界可以作为成核位点。激活<;c + a>;高位错密度区域的位错及其相互作用促进了新晶界的形成和相关SRX的形成。丰富的<;c + a>;基底取向孪晶中的位错释放了压缩孪晶中的应变积累,从而导致SRX的缺失。孪晶尺寸差、存储能和位错-孪晶相互作用是退火过程中脱孪的主要原因。具有高迁移率的近重合点阵边界被认为是SRXed晶粒优先长大的重要因素。
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来源期刊
Journal of Magnesium and Alloys
Journal of Magnesium and Alloys Engineering-Mechanics of Materials
CiteScore
20.20
自引率
14.80%
发文量
52
审稿时长
59 days
期刊介绍: The Journal of Magnesium and Alloys serves as a global platform for both theoretical and experimental studies in magnesium science and engineering. It welcomes submissions investigating various scientific and engineering factors impacting the metallurgy, processing, microstructure, properties, and applications of magnesium and alloys. The journal covers all aspects of magnesium and alloy research, including raw materials, alloy casting, extrusion and deformation, corrosion and surface treatment, joining and machining, simulation and modeling, microstructure evolution and mechanical properties, new alloy development, magnesium-based composites, bio-materials and energy materials, applications, and recycling.
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